(2R,5R)-5-p-bromobenzyl-2-t-butyl-1-t-butyloxycarbonyl-3-methyl-4-imidazolidinone

Base Information

Chemical Name:(2R,5R)-5-p-bromobenzyl-2-t-butyl-1-t-butyloxycarbonyl-3-methyl-4-imidazolidinone
CAS No.:119838-18-5
Molecular Formula:C₂₀H₂₉BrN₂O₃
Molecular Weight:425.366
Hs Code.:

Synonyms:(2R,5R)-5-p-bromobenzyl-2-t-butyl-1-t-butyloxycarbonyl-3-methyl-4-imidazolidinone

Suppliers and Price of (2R,5R)-5-p-bromobenzyl-2-t-butyl-1-t-butyloxycarbonyl-3-methyl-4-imidazolidinone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,5R)-5-p-bromobenzyl-2-t-butyl-1-t-butyloxycarbonyl-3-methyl-4-imidazolidinone

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of (2R,5R)-5-p-bromobenzyl-2-t-butyl-1-t-butyloxycarbonyl-3-methyl-4-imidazolidinone

There total 1 articles about (2R,5R)-5-p-bromobenzyl-2-t-butyl-1-t-butyloxycarbonyl-3-methyl-4-imidazolidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 119838-44-7
tert-butoxycarbonyl-2-(tert-butyl)-3-methyl-4-oxo-1-imidazolidinecarboxylate

: 589-15-1
1-bromomethyl-4-bromobenzene

: 119838-18-5
(2R,5R)-5-p-bromobenzyl-2-t-butyl-1-t-butyloxycarbonyl-3-methyl-4-imidazolidinone

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; hexane; at -75 ℃;
DOI:10.1016/S0040-4020(01)86036-1

Reference yield:

: 119838-18-5
(2R,5R)-5-p-bromobenzyl-2-t-butyl-1-t-butyloxycarbonyl-3-methyl-4-imidazolidinone

: 62561-74-4
(2R)-2-amino-3-(4-bromophenyl)propanoic acid

Guidance literature:: With DOWEX 50 Wx 8 cation exchange resin; trifluoroacetic acid; Yield given. Multistep reaction; 1.) CH₂Cl₂, overnight; 2.) AcOH, 0.75 N HCl, 100 degC, 44 h;
DOI:10.1016/S0040-4020(01)86036-1