C₂₄H₄₄O₃Si

Base Information

Chemical Name:C₂₄H₄₄O₃Si
CAS No.:1322669-24-8
Molecular Formula:C₂₄H₄₄O₃Si
Molecular Weight:408.697
Hs Code.:

C<sub>24</sub>H<sub>44</sub>O<sub>3</sub>Si

Synonyms:C₂₄H₄₄O₃Si

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Chemical Property of C₂₄H₄₄O₃Si

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Technology Process of C₂₄H₄₄O₃Si

There total 11 articles about C₂₄H₄₄O₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1322669-23-7
(2R,3R,4R,5R,6R)-3-(benzyloxy)-5-[1-(tert-butyl)-1,1-dimethylsilyl]oxy-2,4-dimethyl-6-([(4-methylphenyl)sulfonyl]oxymethyl)octyl pivalate

: 1322669-24-8
C₂₄H₄₄O₃Si

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 20 ℃; for 4h;
DOI:10.1016/j.tetlet.2011.05.151

Reference yield:

: 1322669-21-5
C₁₈H₂₄O₄

: 1322669-24-8
C₂₄H₄₄O₃Si

Guidance literature:: Multi-step reaction with 7 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / 0 - 20 °C

2: pyridinium p-toluenesulfonate / dichloromethane / 12 h / 0 - 20 °C

3: triethylamine / dichloromethane / 12 h / 0 - 20 °C

4: toluene-4-sulfonic acid / methanol / 10 h / 0 - 20 °C

5: di(n-butyl)tin oxide; triethylamine / dichloromethane / 10 h / 0 - 20 °C

6: 2,6-dimethylpyridine / dichloromethane / 1 h / 0 - 20 °C

7: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / 0 - 20 °C

With 2,6-dimethylpyridine; lithium aluminium tetrahydride; pyridinium p-toluenesulfonate; di(n-butyl)tin oxide; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.tetlet.2011.05.151

Reference yield:

: 1322669-27-1
C₂₁H₃₄O₄

: 1322669-24-8
C₂₄H₄₄O₃Si

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine / dichloromethane / 12 h / 0 - 20 °C

2: toluene-4-sulfonic acid / methanol / 10 h / 0 - 20 °C

3: di(n-butyl)tin oxide; triethylamine / dichloromethane / 10 h / 0 - 20 °C

4: 2,6-dimethylpyridine / dichloromethane / 1 h / 0 - 20 °C

5: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / 0 - 20 °C

With 2,6-dimethylpyridine; lithium aluminium tetrahydride; di(n-butyl)tin oxide; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.tetlet.2011.05.151