C₃₀H₃₄O₁₂S₂

Base Information

Chemical Name:C₃₀H₃₄O₁₂S₂
CAS No.:1053245-48-9
Molecular Formula:C₃₀H₃₄O₁₂S₂
Molecular Weight:650.725
Hs Code.:

C<sub>30</sub>H<sub>34</sub>O<sub>12</sub>S<sub>2</sub>

Synonyms:C₃₀H₃₄O₁₂S₂

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Chemical Property of C₃₀H₃₄O₁₂S₂

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Technology Process of C₃₀H₃₄O₁₂S₂

There total 7 articles about C₃₀H₃₄O₁₂S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 325794-16-9
(1R,2R,3R,5R,7R)-7-((R)-1,2-Dihydroxy-ethyl)-5-(3,4-dimethoxy-phenyl)-6,8-dioxa-bicyclo[3.2.1]octane-2,3-diol

: 1053245-48-9
C₃₀H₃₄O₁₂S₂

Guidance literature:: With triethylamine; di(n-butyl)tin oxide; In dichloromethane; at 20 ℃; for 16h;
DOI:10.1021/ol006887l

Reference yield:

: 91-16-7
1,2-dimethoxybenzene

: 1053245-48-9
C₃₀H₃₄O₁₂S₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: 75 percent / AlCl₃ / CH₂Cl₂ / 3 h / 0 °C

2.1: 90 percent / CSA / benzene / 12 h / Heating

3.1: o-NO₂PhSeCN; NaBH₄ / ethanol; H₂O / 0 - 20 °C

3.2: 96 percent / H₂O₂ / tetrahydrofuran / 20 °C

4.1: 91 percent / PhCH=Ru(PCy₃)2Cl₂ / benzene / 1.5 h / Heating

5.1: 94 percent / (DHQ)2AQN; OsO₄; K₂CO₃ / K₃Fe(CN)6 / 2-methyl-propan-2-ol; H₂O / 31 h / 0 °C

6.1: Et₃N / Bu₂Sn=O / CH₂Cl₂ / 16 h / 20 °C

With sodium tetrahydroborate; osmium(VIII) oxide; aluminium trichloride; ortho-nitrophenyl selenocyanate; (DHQ)2AQN; camphor-10-sulfonic acid; potassium carbonate; triethylamine; Grubbs catalyst first generation; di(n-butyl)tin oxide; potassium hexacyanoferrate(III); In ethanol; dichloromethane; water; tert-butyl alcohol; benzene; 3.2: Sharpless' procedure;
DOI:10.1021/ol006887l

Reference yield:

: 1069-23-4,19700-96-0,19700-97-1,58208-04-1,144829-86-7,112571-38-7
(3R,4R)-1,5-hexadiene-3,4-diol

: 1053245-48-9
C₃₀H₃₄O₁₂S₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: 90 percent / CSA / benzene / 12 h / Heating

2.1: o-NO₂PhSeCN; NaBH₄ / ethanol; H₂O / 0 - 20 °C

2.2: 96 percent / H₂O₂ / tetrahydrofuran / 20 °C

3.1: 91 percent / PhCH=Ru(PCy₃)2Cl₂ / benzene / 1.5 h / Heating

4.1: 94 percent / (DHQ)2AQN; OsO₄; K₂CO₃ / K₃Fe(CN)6 / 2-methyl-propan-2-ol; H₂O / 31 h / 0 °C

5.1: Et₃N / Bu₂Sn=O / CH₂Cl₂ / 16 h / 20 °C

With sodium tetrahydroborate; osmium(VIII) oxide; ortho-nitrophenyl selenocyanate; (DHQ)2AQN; camphor-10-sulfonic acid; potassium carbonate; triethylamine; Grubbs catalyst first generation; di(n-butyl)tin oxide; potassium hexacyanoferrate(III); In ethanol; dichloromethane; water; tert-butyl alcohol; benzene; 2.2: Sharpless' procedure;
DOI:10.1021/ol006887l