meso-dibutenanilide

Base Information

Chemical Name:meso-dibutenanilide
CAS No.:454450-86-3
Molecular Formula:C₇₄H₇₂F₆N₈O₁₂S₄
Molecular Weight:1507.69
Hs Code.:

Synonyms:meso-dibutenanilide

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Chemical Property of meso-dibutenanilide

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Technology Process of meso-dibutenanilide

There total 1 articles about meso-dibutenanilide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 688-73-3
tri-n-butyl-tin hydride

: 454450-84-1
meso-7,7'-diiodo-1,1'-dimethyl-1,2,3,8,8a,1',2',3',8',8a'-octahydro-1H,1'H-[3a,3a']bi[pyrrolo[2,3-b]indolyl]

: 454450-91-0
trifluoromethanesulfonic acid 2-(benzyl-4{4-[methyl-(toluene-4-sulfonyl)-amino]-but-2-ynoyl}-amino)-phenyl ester

: 454450-86-3
meso-dibutenanilide

Guidance literature:: tri-n-butyl-tin hydride; trifluoromethanesulfonic acid 2-(benzyl-4{4-[methyl-(toluene-4-sulfonyl)-amino]-but-2-ynoyl}-amino)-phenyl ester; With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; copper(l) iodide; trifuran-2-yl-phosphane; In 1-methyl-pyrrolidin-2-one; at 0 - 20 ℃; for 2.66667h;

meso-7,7'-diiodo-1,1'-dimethyl-1,2,3,8,8a,1',2',3',8',8a'-octahydro-1H,1'H-[3a,3a']bi[pyrrolo[2,3-b]indolyl]; copper(l) iodide; phosphan; palladium; Further stages.;
DOI:10.1021/ja0267425

Reference yield:

: 454450-86-3
meso-dibutenanilide

: C₇₂H₇₀N₈O₆S₂

: C₇₂H₇₀N₈O₆S₂

: (3aS,3a'R,3a''S,3a'''S,8aS,8a'R)-dioxindole

: C₇₂H₇₀N₈O₆S₂

Guidance literature:: With 1,2,2,6,6-pentamethylpiperidine; palladium diacetate; (R)-tol-BINAP; In acetonitrile; at 80 ℃; for 12h; Title compound not separated from byproducts.;
DOI:10.1021/ja0267425