N-Acetyl-N-hydroxy-2-phenylacetamide

Base Information

• Chemical Name: N-Acetyl-N-hydroxy-2-phenylacetamide
• CAS No.: 77130-75-7
• Molecular Formula: C10H11 N O3
• Molecular Weight: 193.2
• Hs Code.: 2925190090
• DSSTox Substance ID: DTXSID60504130
• Wikidata: Q82358409
• Mol file: 77130-75-7.mol

Synonyms:N-ACETYL-N-HYDROXY-2-PHENYLACETAMIDE;77130-75-7;N-Hydroxy-N-phenylacetyl-acetamide;DTXSID60504130;AKOS006295631;SB38681;FT-0693703;A838967

Chemical Property of N-Acetyl-N-hydroxy-2-phenylacetamide

Chemical Property:

• PSA: 57.61000
• LogP: 0.99340
• XLogP3: 0.6
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 2
• Exact Mass: 193.07389321
• Heavy Atom Count: 14
• Complexity: 221

Purity/Quality:

97% ^*data from raw suppliers

n-acetyl-n-hydroxy-2-phenylacetamide 95 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=O)N(C(=O)CC1=CC=CC=C1)O

Technology Process of N-Acetyl-N-hydroxy-2-phenylacetamide

There total 5 articles about N-Acetyl-N-hydroxy-2-phenylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

acide N-acetyl chloro-2 phenyl-2 acetohydroxamique (77130-74-6) → acide N-acetyl phenyl-2 acetohydroxamique (77130-75-7)

Guidance literature:

With tri-n-butyl-tin hydride; In toluene; at 80 ℃; for 6h;

DOI:10.1016/0040-4020(80)80224-9

Reference yield:

N-Acetyl-O-benzyl-N-phenylacetyl-hydroxylamin (22426-99-9) → acide N-acetyl phenyl-2 acetohydroxamique (77130-75-7)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; Ambient temperature;

DOI:10.1016/S0040-4039(01)80290-2

Reference yield:

N-(benzyloxy)-2-phenylacetamide (22426-86-4) → acide N-acetyl phenyl-2 acetohydroxamique (77130-75-7)

Guidance literature:

Multi-step reaction with 2 steps

1: BuLi

2: H₂ / Pd/C / methanol / Ambient temperature

With n-butyllithium; hydrogen; palladium on activated charcoal; In methanol;

DOI:10.1016/S0040-4039(01)80290-2

upstream raw materials:

N-Acetyl-O-benzyl-N-phenylacetyl-hydroxylamin

acide N-acetyl chloro-2 phenyl-2 acetohydroxamique

N-(benzyloxy)-2-phenylacetamide

phenylacetyl chloride

Downstream raw materials:

anhydride N-acetyl phenyl-acetohydroxamique-acetique

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