(Z)-2-Phenyl-3,3a,4,5,6,9,10,11-octahydro-2H-1-oxa-11a-aza-cyclopentacyclodecene

Base Information

Chemical Name:(Z)-2-Phenyl-3,3a,4,5,6,9,10,11-octahydro-2H-1-oxa-11a-aza-cyclopentacyclodecene
CAS No.:98218-77-0
Molecular Formula:C₁₇H₂₃NO
Molecular Weight:257.376
Hs Code.:

Synonyms:(Z)-2-Phenyl-3,3a,4,5,6,9,10,11-octahydro-2H-1-oxa-11a-aza-cyclopentacyclodecene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-2-Phenyl-3,3a,4,5,6,9,10,11-octahydro-2H-1-oxa-11a-aza-cyclopentacyclodecene

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Technology Process of (Z)-2-Phenyl-3,3a,4,5,6,9,10,11-octahydro-2H-1-oxa-11a-aza-cyclopentacyclodecene

There total 8 articles about (Z)-2-Phenyl-3,3a,4,5,6,9,10,11-octahydro-2H-1-oxa-11a-aza-cyclopentacyclodecene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 98218-74-7
1-hydroxy-cis,cis-5-<(p-tolylsulfonyl)oxy>decahydroquinoline

: 98218-77-0
(Z)-2-Phenyl-3,3a,4,5,6,9,10,11-octahydro-2H-1-oxa-11a-aza-cyclopentacyclodecene

Guidance literature:: With sodium hydride; In tetrahydrofuran; for 24h;
DOI:10.1021/jo00220a057

Reference yield:

: 53400-41-2
5,6,7,8-tetrahydroquinolin-5-one

: 98218-77-0
(Z)-2-Phenyl-3,3a,4,5,6,9,10,11-octahydro-2H-1-oxa-11a-aza-cyclopentacyclodecene

Guidance literature:: Multi-step reaction with 6 steps

1: 94 percent / NaBH₄ / methanol

2: 36 percent / H₂, PtO₂ / acetic acid; methanol / 3361.5 Torr

3: 95 percent

4: 99 percent / DMAP / CH₂Cl₂

5: 84 percent / MCPBA / CH₂Cl₂

6: 59 percent / NaH / tetrahydrofuran / 24 h

With dmap; platinum(IV) oxide; sodium tetrahydroborate; hydrogen; sodium hydride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; dichloromethane; acetic acid;
DOI:10.1021/jo00220a057

Reference yield:

: 194151-99-0
5,6,7,8-tetrahydroquinolin-5-ol

: 98218-77-0
(Z)-2-Phenyl-3,3a,4,5,6,9,10,11-octahydro-2H-1-oxa-11a-aza-cyclopentacyclodecene

Guidance literature:: Multi-step reaction with 5 steps

1: 36 percent / H₂, PtO₂ / acetic acid; methanol / 3361.5 Torr

2: 95 percent

3: 99 percent / DMAP / CH₂Cl₂

4: 84 percent / MCPBA / CH₂Cl₂

5: 59 percent / NaH / tetrahydrofuran / 24 h

With dmap; platinum(IV) oxide; hydrogen; sodium hydride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; dichloromethane; acetic acid;
DOI:10.1021/jo00220a057