HFeRu₃N(CO)11(P(OCH₃)3)

Base Information

• Chemical Name: HFeRu₃N(CO)11(P(OCH₃)3)
• CAS No.: 100927-56-8
• Molecular Formula: C₁₄H₁₀FeNO₁₄PRu₃
• Molecular Weight: 806.262
• Mol file: 100927-56-8.mol

Synonyms:HFeRu₃N(CO)11(P(OCH₃)3)

Chemical Property of HFeRu₃N(CO)11(P(OCH₃)3)

Chemical Property:

Purity/Quality:

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Technology Process of HFeRu₃N(CO)11(P(OCH₃)3)

There total 1 articles about HFeRu₃N(CO)11(P(OCH₃)3) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

(P(C6H5)3NP(C6H5)3)(1+)*[FeRu3N(CO)10(P(OCH3)3)2](1-)=(P(C6H5)3NP(C6H5)3)[FeRu3N(CO)10(P(OCH3)3)2] (100927-53-5) + trifluorormethanesulfonic acid (1493-13-6) → dodecacarbonyl-triangulo-triruthenium (15243-33-1) + FeRu2(NH)(CO)9(P(OCH3)3) (100938-66-7) + HFeRu3N(CO)11(P(OCH3)3) (100927-56-8) + HFeRu3N(CO)10(P(OCH3)3)2 (100938-64-5)

Guidance literature:

With CO; In dichloromethane; CH2Cl2 was distilled into tube contg. of PPN(FeRu3N(CO)10(P(OMe)3)2), CO was bubbled through the soln. for 10 min, CF3SO3H was added; the volume was reduced, oil was extd. with hexane, filtrate was chromd.; elem. anal.;

DOI:10.1021/ja00269a028

upstream raw materials:

(P(C₆H₅)3NP(C₆H₅)3)⁽¹⁺⁾*[FeRu₃N(CO)10(P(OCH₃)3)2]^(1-)=(P(C₆H₅)3NP(C₆H₅)3)[FeRu₃N(CO)10(P(OCH₃)3)2]

trifluorormethanesulfonic acid