dichloro(bis(2-isopropylamino-4-methoxyphenyl)amine(-3H))tantalum(V)

Base Information

• Chemical Name: dichloro(bis(2-isopropylamino-4-methoxyphenyl)amine(-3H))tantalum(V)
• CAS No.: 1133239-24-3
• Molecular Formula: C₂₀H₂₆Cl₂N₃O₂Ta
• Molecular Weight: 592.299

Synonyms:dichloro(bis(2-isopropylamino-4-methoxyphenyl)amine(-3H))tantalum(V)

Chemical Property of dichloro(bis(2-isopropylamino-4-methoxyphenyl)amine(-3H))tantalum(V)

Chemical Property:

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Technology Process of dichloro(bis(2-isopropylamino-4-methoxyphenyl)amine(-3H))tantalum(V)

There total 1 articles about dichloro(bis(2-isopropylamino-4-methoxyphenyl)amine(-3H))tantalum(V) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dichloro(bis(2-isopropylamino-4-methoxyphenyl)amine(1-))(phenylimido)tantalum(V) → (N(C6H3(OCH3)NCH(CH3)2)2)TaCl2 (1133239-24-3) + (N(C6H3(OCH3)NCH(CH3)2)2)TaCl2(NHC6H5)

Guidance literature:

With 1,2-diphenylhydrazine; In tetrahydrofuran; byproducts: aniline, azobenze; using standard Schlenk techniques; PhNHNHPh (excess) added to Ta complexin THF at 35°C; monitored by UV-vis spectra;

DOI:10.1021/ic200911b

Reference yield: 99.0%

dichloro(bis(2-isopropylamino-4-methoxyphenyl)amine(-3H))tantalum(V) (1133239-24-3) + N-benzyl-N,N,N-triethylammonium chloride (56-37-1) → C20H26Cl3N3O2Ta(1-)*C13H22N(1+)

Guidance literature:

In tetrahydrofuran; for 12h; Inert atmosphere;

DOI:10.1021/ic401496w

Reference yield: 97.0%

p-methylazidobenzene (2101-86-2) + dichloro(bis(2-isopropylamino-4-methoxyphenyl)amine(-3H))tantalum(V) (1133239-24-3) → dichloro(bis(2-isopropylamino-4-methoxyphenyl)amine(1-))(p-tolylimido)tantalum(V)

Guidance literature:

In toluene; byproducts: N2; under Ar or N2; soln. of Ta complex in toluene treated with MeC6H5N3 at room temp.; stirred for 12 h; ppt. collected by filtration; washed with cyclopentane; elem. anal.;

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