(3aR,5R,6R,6aR)-6-benzyloxy-2,2-dimethyl-5-vinyl-5-[(1S)-1-benzyloxybut-3-enyl]tetrahydrofuro[2,3-d][1,3]dioxole

Base Information

• Chemical Name: (3aR,5R,6R,6aR)-6-benzyloxy-2,2-dimethyl-5-vinyl-5-[(1S)-1-benzyloxybut-3-enyl]tetrahydrofuro[2,3-d][1,3]dioxole
• CAS No.: 1253800-20-2
• Molecular Formula: C₂₇H₃₂O₅
• Molecular Weight: 436.548

Synonyms:(3aR,5R,6R,6aR)-6-benzyloxy-2,2-dimethyl-5-vinyl-5-[(1S)-1-benzyloxybut-3-enyl]tetrahydrofuro[2,3-d][1,3]dioxole

Chemical Property of (3aR,5R,6R,6aR)-6-benzyloxy-2,2-dimethyl-5-vinyl-5-[(1S)-1-benzyloxybut-3-enyl]tetrahydrofuro[2,3-d][1,3]dioxole

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Technology Process of (3aR,5R,6R,6aR)-6-benzyloxy-2,2-dimethyl-5-vinyl-5-[(1S)-1-benzyloxybut-3-enyl]tetrahydrofuro[2,3-d][1,3]dioxole

There total 1 articles about (3aR,5R,6R,6aR)-6-benzyloxy-2,2-dimethyl-5-vinyl-5-[(1S)-1-benzyloxybut-3-enyl]tetrahydrofuro[2,3-d][1,3]dioxole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

(3aR,5S,6R,6aR)-6-benzyloxy-2,2-dimethyl-5-vinyl-5-[(1S)-1-hydroxybut-3-enyl]tetrahydrofuro[2,3-d][1,3]dioxole (1253800-18-8) + benzyl bromide (100-39-0) → (3aR,5R,6R,6aR)-6-benzyloxy-2,2-dimethyl-5-vinyl-5-[(1S)-1-benzyloxybut-3-enyl]tetrahydrofuro[2,3-d][1,3]dioxole (1253800-20-2)

Guidance literature:

(3aR,5S,6R,6aR)-6-benzyloxy-2,2-dimethyl-5-vinyl-5-[(1S)-1-hydroxybut-3-enyl]tetrahydrofuro[2,3-d][1,3]dioxole; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.0833333h;

benzyl bromide; With tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; at 20 ℃; for 2h;

DOI:10.1055/s-0029-1218828

Reference yield: 70.0%

(3aR,5R,6R,6aR)-6-benzyloxy-2,2-dimethyl-5-vinyl-5-[(1S)-1-benzyloxybut-3-enyl]tetrahydrofuro[2,3-d][1,3]dioxole (1253800-20-2) → C25H28O5 (1253800-21-3)

Guidance literature:

With Grubbs catalyst first generation; In benzene; for 45h; Inert atmosphere; Reflux;

DOI:10.1055/s-0029-1218828

upstream raw materials:

(3aR,5S,6R,6aR)-6-benzyloxy-2,2-dimethyl-5-vinyl-5-[(1S)-1-hydroxybut-3-enyl]tetrahydrofuro[2,3-d][1,3]dioxole

benzyl bromide

Downstream raw materials:

C₂₅H₂₈O₅

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