4-((4-(2-aminothiazol-5-yl)-6-morpholino-1,3,5-triazin-2-yl)oxy)-N,N′-dimethylbenzamide hydrochloride

Base Information

Chemical Name:4-((4-(2-aminothiazol-5-yl)-6-morpholino-1,3,5-triazin-2-yl)oxy)-N,N′-dimethylbenzamide hydrochloride
CAS No.:1391926-30-9
Molecular Formula:C₁₉H₂₁N₇O₃S*ClH
Molecular Weight:463.948
Hs Code.:

Synonyms:4-((4-(2-aminothiazol-5-yl)-6-morpholino-1,3,5-triazin-2-yl)oxy)-N,N′-dimethylbenzamide hydrochloride

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Chemical Property of 4-((4-(2-aminothiazol-5-yl)-6-morpholino-1,3,5-triazin-2-yl)oxy)-N,N′-dimethylbenzamide hydrochloride

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Technology Process of 4-((4-(2-aminothiazol-5-yl)-6-morpholino-1,3,5-triazin-2-yl)oxy)-N,N′-dimethylbenzamide hydrochloride

There total 8 articles about 4-((4-(2-aminothiazol-5-yl)-6-morpholino-1,3,5-triazin-2-yl)oxy)-N,N′-dimethylbenzamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1391926-40-1
tert-butyl (5-(4-(4-(dimethylcarbamoyl)phenoxy)-6-morpholino-1,3,5-triazin-2-yl)thiazol-2-yl)carbamate

: 1391926-30-9
4-((4-(2-aminothiazol-5-yl)-6-morpholino-1,3,5-triazin-2-yl)oxy)-N,N′-dimethylbenzamide hydrochloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 24h;

Reference yield:

: 6601-22-5
2,6-Dichloro-4-morpholino-1,3,5-triazine

: 1391926-30-9
4-((4-(2-aminothiazol-5-yl)-6-morpholino-1,3,5-triazin-2-yl)oxy)-N,N′-dimethylbenzamide hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydrogencarbonate / water; acetone / 2 h / 20 °C

2: bis-triphenylphosphine-palladium(II) chloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 16 h / 95 °C / Inert atmosphere

3: hydrogenchloride / 1,4-dioxane / 24 h / 20 °C

With hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; water; N,N-dimethyl-formamide; acetone;

Reference yield:

: 1391926-57-0
C₁₆H₁₈ClN₅O₃

: 1391926-30-9
4-((4-(2-aminothiazol-5-yl)-6-morpholino-1,3,5-triazin-2-yl)oxy)-N,N′-dimethylbenzamide hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: bis-triphenylphosphine-palladium(II) chloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 16 h / 95 °C / Inert atmosphere

2: hydrogenchloride / 1,4-dioxane / 24 h / 20 °C

With hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; N,N-dimethyl-formamide;