(1R,5S,7R)-1,5,7-Tris-benzyloxymethyl-2,4-dioxo-3-aza-bicyclo[3.3.1]nonane-7-carboxylic acid naphthalen-2-ylamide

Base Information

Chemical Name:(1R,5S,7R)-1,5,7-Tris-benzyloxymethyl-2,4-dioxo-3-aza-bicyclo[3.3.1]nonane-7-carboxylic acid naphthalen-2-ylamide
CAS No.:146651-56-1
Molecular Formula:C₄₃H₄₂N₂O₆
Molecular Weight:682.816
Hs Code.:

Synonyms:(1R,5S,7R)-1,5,7-Tris-benzyloxymethyl-2,4-dioxo-3-aza-bicyclo[3.3.1]nonane-7-carboxylic acid naphthalen-2-ylamide

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Chemical Property of (1R,5S,7R)-1,5,7-Tris-benzyloxymethyl-2,4-dioxo-3-aza-bicyclo[3.3.1]nonane-7-carboxylic acid naphthalen-2-ylamide

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Technology Process of (1R,5S,7R)-1,5,7-Tris-benzyloxymethyl-2,4-dioxo-3-aza-bicyclo[3.3.1]nonane-7-carboxylic acid naphthalen-2-ylamide

There total 7 articles about (1R,5S,7R)-1,5,7-Tris-benzyloxymethyl-2,4-dioxo-3-aza-bicyclo[3.3.1]nonane-7-carboxylic acid naphthalen-2-ylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17690-16-3
benzyl bromomethyl ether

: 146651-56-1
(1R,5S,7R)-1,5,7-Tris-benzyloxymethyl-2,4-dioxo-3-aza-bicyclo[3.3.1]nonane-7-carboxylic acid naphthalen-2-ylamide

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) LDA

2: KOH / ethanol / Heating

3: xylene / Heating

4: aq. NH₃

5: SOCl₂

6: pyridine

With pyridine; potassium hydroxide; ammonium hydroxide; thionyl chloride; lithium diisopropyl amide; In ethanol; xylene;
DOI:10.1021/ja00055a066

Reference yield:

: 52831-11-5
trimethyl cyclohexane-1,3,5-tricarboxylate

: 146651-56-1
(1R,5S,7R)-1,5,7-Tris-benzyloxymethyl-2,4-dioxo-3-aza-bicyclo[3.3.1]nonane-7-carboxylic acid naphthalen-2-ylamide

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) LDA

2: KOH / ethanol / Heating

3: xylene / Heating

4: aq. NH₃

5: SOCl₂

6: pyridine

With pyridine; potassium hydroxide; ammonium hydroxide; thionyl chloride; lithium diisopropyl amide; In ethanol; xylene;
DOI:10.1021/ja00055a066

Reference yield:

: 146651-50-5
1,3,5-Tris-benzyloxymethyl-cyclohexane-1,3,5-tricarboxylic acid trimethyl ester

: 146651-56-1
(1R,5S,7R)-1,5,7-Tris-benzyloxymethyl-2,4-dioxo-3-aza-bicyclo[3.3.1]nonane-7-carboxylic acid naphthalen-2-ylamide

Guidance literature:: Multi-step reaction with 5 steps

1: KOH / ethanol / Heating

2: xylene / Heating

3: aq. NH₃

4: SOCl₂

5: pyridine

With pyridine; potassium hydroxide; ammonium hydroxide; thionyl chloride; In ethanol; xylene;
DOI:10.1021/ja00055a066