C₂₅H₂₆N₂O₄

Base Information

Chemical Name:C₂₅H₂₆N₂O₄
CAS No.:853072-54-5
Molecular Formula:C₂₅H₂₆N₂O₄
Molecular Weight:418.492
Hs Code.:

C<sub>25</sub>H<sub>26</sub>N<sub>2</sub>O<sub>4</sub>

Synonyms:C₂₅H₂₆N₂O₄

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Chemical Property of C₂₅H₂₆N₂O₄

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Technology Process of C₂₅H₂₆N₂O₄

There total 8 articles about C₂₅H₂₆N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 474302-74-4
trans-(1S,3R)-(-)-2-benzyl-3-ethoxycarbonyl-7-methoxy-1-methoxycarbonylethyl-9-methyl-1,2,3,4-tetrahydro-9H-pyrido[3,4-b]indole

: 853072-54-5
C₂₅H₂₆N₂O₄

Guidance literature:: With sodium hydride; In methanol; toluene; for 4h; Heating;
DOI:10.1021/jo040282b

Reference yield:

: 153898-63-6
2-iodo-5-methoxyaniline

: 853072-54-5
C₂₅H₂₆N₂O₄

Guidance literature:: Multi-step reaction with 6 steps

1.1: 77 percent / lithium chloride; sodium carbonate / palladium(II) acetate / dimethylformamide / 36 h / 100 °C

2.1: 95 percent / sodium hydride / dimethylformamide; various solvent(s) / 2 h / 0 °C

3.1: 93 percent / HCl / tetrahydrofuran; H₂O / 0 - 20 °C

4.1: ethanol / 5 h / 20 °C

4.2: 93 percent / NaBH₄ / ethanol / 4 h / -10 - -5 °C

5.1: acetic acid / CH₂Cl₂ / 0 - 20 °C

5.2: 90 percent / TFA / CH₂Cl₂ / 12 h / 20 °C

6.1: 85 percent / sodium hydride / toluene; various solvent(s); methanol / 4 h / Heating

With hydrogenchloride; sodium hydride; sodium carbonate; acetic acid; lithium chloride; palladium diacetate; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; 1.1: Larock heteroannulation / 5.1: Pictet-Spengler condensation / 6.1: Dieckmann cyclization;
DOI:10.1021/jo040282b

Reference yield:

: 355839-49-5
(2S,5R)-3,6-diethoxy-2-isopropyl-5-[3-(triethylsilyl)prop-2-ynyl]-2,5-dihydropyrazine

: 853072-54-5
C₂₅H₂₆N₂O₄

Guidance literature:: Multi-step reaction with 6 steps

1.1: 77 percent / lithium chloride; sodium carbonate / palladium(II) acetate / dimethylformamide / 36 h / 100 °C

2.1: 95 percent / sodium hydride / dimethylformamide; various solvent(s) / 2 h / 0 °C

3.1: 93 percent / HCl / tetrahydrofuran; H₂O / 0 - 20 °C

4.1: ethanol / 5 h / 20 °C

4.2: 93 percent / NaBH₄ / ethanol / 4 h / -10 - -5 °C

5.1: acetic acid / CH₂Cl₂ / 0 - 20 °C

5.2: 90 percent / TFA / CH₂Cl₂ / 12 h / 20 °C

6.1: 85 percent / sodium hydride / toluene; various solvent(s); methanol / 4 h / Heating

With hydrogenchloride; sodium hydride; sodium carbonate; acetic acid; lithium chloride; palladium diacetate; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; 1.1: Larock heteroannulation / 5.1: Pictet-Spengler condensation / 6.1: Dieckmann cyclization;
DOI:10.1021/jo040282b