methyl N-[2-(benzyloxy)ethyl]-N-[7-(F-octyl)heptyl]-11-carboxamidoundecanoate

Base Information

Chemical Name:methyl N-[2-(benzyloxy)ethyl]-N-[7-(F-octyl)heptyl]-11-carboxamidoundecanoate
CAS No.:350689-56-4
Molecular Formula:C₃₇H₄₈F₁₇NO₄
Molecular Weight:893.765
Hs Code.:

Synonyms:methyl N-[2-(benzyloxy)ethyl]-N-[7-(F-octyl)heptyl]-11-carboxamidoundecanoate

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Chemical Property of methyl N-[2-(benzyloxy)ethyl]-N-[7-(F-octyl)heptyl]-11-carboxamidoundecanoate

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Technology Process of methyl N-[2-(benzyloxy)ethyl]-N-[7-(F-octyl)heptyl]-11-carboxamidoundecanoate

There total 5 articles about methyl N-[2-(benzyloxy)ethyl]-N-[7-(F-octyl)heptyl]-11-carboxamidoundecanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 3903-40-0
12-methoxy-12-oxododecanoic acid

: 350689-58-6
N-[2-(benzyloxy)ethyl]-7-(F-octyl)heptylamine

: 350689-56-4
methyl N-[2-(benzyloxy)ethyl]-N-[7-(F-octyl)heptyl]-11-carboxamidoundecanoate

Guidance literature:: With triethylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/jm0011124

Reference yield:

: 10471-28-0
diethyl dodecanedioate

: 350689-56-4
methyl N-[2-(benzyloxy)ethyl]-N-[7-(F-octyl)heptyl]-11-carboxamidoundecanoate

Guidance literature:: Multi-step reaction with 2 steps

1: Ba(OH)2

2: 78 percent / PyBrop; Et₃N / CH₂Cl₂ / 0 - 20 °C

With barium dihydroxide; triethylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; In dichloromethane;
DOI:10.1021/jm0011124

Reference yield:

: 10578-75-3
2-(phenylmethoxy)-ethylamine hydrochloride

: 350689-56-4
methyl N-[2-(benzyloxy)ethyl]-N-[7-(F-octyl)heptyl]-11-carboxamidoundecanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / Et₃N; HOBt; EDC / CH₂Cl₂ / 0 - 20 °C

2: 80 percent / LiAlH₄ / tetrahydrofuran / 24 h / 20 °C

3: 78 percent / PyBrop; Et₃N / CH₂Cl₂ / 0 - 20 °C

With lithium aluminium tetrahydride; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm0011124