methyl (4-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-2,4-di-O-benzyl-α-L-rhamnopyranoside

Base Information

Chemical Name:methyl (4-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-2,4-di-O-benzyl-α-L-rhamnopyranoside
CAS No.:144174-64-1
Molecular Formula:C₃₄H₄₂O₉
Molecular Weight:594.702
Hs Code.:

Synonyms:methyl (4-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-2,4-di-O-benzyl-α-L-rhamnopyranoside

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Chemical Property of methyl (4-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-2,4-di-O-benzyl-α-L-rhamnopyranoside

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Technology Process of methyl (4-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-2,4-di-O-benzyl-α-L-rhamnopyranoside

There total 11 articles about methyl (4-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-2,4-di-O-benzyl-α-L-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 294677-67-1
methyl (2,3-di-O-acetyl-4-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-2,4-di-O-benzyl-α-L-rhamnopyranoside

: 144174-64-1
methyl (4-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-2,4-di-O-benzyl-α-L-rhamnopyranoside

Guidance literature:: With sodium methylate; In methanol; dichloromethane; at 20 ℃; for 15h; pH=10;
DOI:10.1080/07328300008544096

Reference yield: 85.0%

: 144174-63-0
Methyl 2,4-di-O-benzyl-3-O-(4-O-benzyl-2,3-O-isopropylidene-α-L-rhamnopyranosyl)-α-L-rhamnopyranoside

: 144174-64-1
methyl (4-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-2,4-di-O-benzyl-α-L-rhamnopyranoside

Guidance literature:: With acetic acid; at 70 ℃; for 18h;
DOI:10.1016/0008-6215(93)84227-W

Reference yield:

: 100-39-0
benzyl bromide

: 144174-64-1
methyl (4-O-benzyl-α-L-rhamnopyranosyl)-(1->3)-2,4-di-O-benzyl-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / NaH / paraffin; tetrahydrofuran / 18 h

2: 85 percent / aq. 70percent acetic acid / 18 h / 70 °C

With sodium hydride; acetic acid; In tetrahydrofuran; paraffin;
DOI:10.1016/0008-6215(93)84227-W