2,4-bis(N,N-dimethylaminomethyleneamino)-6-benzenesulfonyloxypteridine

Base Information

Chemical Name:2,4-bis(N,N-dimethylaminomethyleneamino)-6-benzenesulfonyloxypteridine
CAS No.:1422390-71-3
Molecular Formula:C₁₈H₂₀N₈O₃S
Molecular Weight:428.475
Hs Code.:

Synonyms:2,4-bis(N,N-dimethylaminomethyleneamino)-6-benzenesulfonyloxypteridine

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Chemical Property of 2,4-bis(N,N-dimethylaminomethyleneamino)-6-benzenesulfonyloxypteridine

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Technology Process of 2,4-bis(N,N-dimethylaminomethyleneamino)-6-benzenesulfonyloxypteridine

There total 2 articles about 2,4-bis(N,N-dimethylaminomethyleneamino)-6-benzenesulfonyloxypteridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 98-09-9
benzenesulfonyl chloride

: 213739-01-6
2,4-bis(N,N-dimethylaminomethyleneamino)pteridin-6-one

: 1422390-71-3
2,4-bis(N,N-dimethylaminomethyleneamino)-6-benzenesulfonyloxypteridine

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃; for 1h;
DOI:10.3987/COM-12-12610

Reference yield:

: 1917-45-9
2,4-diaminopteridin-6-one

: 1422390-71-3
2,4-bis(N,N-dimethylaminomethyleneamino)-6-benzenesulfonyloxypteridine

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide / 3 h / 65 °C / Inert atmosphere

2: triethylamine; dmap / dichloromethane / 1 h / 0 - 20 °C

With dmap; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.3987/COM-12-12610

Reference yield: 74.0%

: 1422390-71-3
2,4-bis(N,N-dimethylaminomethyleneamino)-6-benzenesulfonyloxypteridine

: 536-74-3
phenylacetylene

: 1426333-64-3
2,4-bis(N,N-dimethylaminomethyleneamino)-6-(phenylethynyl)pteridine

: 1426333-65-4
4-amino-2-(N,N-dimethylaminomethyleneamino)-6-(phenylethynyl)pteridine

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In N,N-dimethyl-formamide; at 80 ℃; for 2h; Overall yield = 650 mg; Inert atmosphere;
DOI:10.3987/COM-12-12610