7-Benzyloxy-hept-1-ene-3,5-diol

Base Information

Chemical Name:7-Benzyloxy-hept-1-ene-3,5-diol
CAS No.:868381-43-5
Molecular Formula:C₁₄H₂₀O₃
Molecular Weight:236.311
Hs Code.:

Synonyms:7-Benzyloxy-hept-1-ene-3,5-diol

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Chemical Property of 7-Benzyloxy-hept-1-ene-3,5-diol

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Technology Process of 7-Benzyloxy-hept-1-ene-3,5-diol

There total 6 articles about 7-Benzyloxy-hept-1-ene-3,5-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: Acetic acid (E)-7-benzyloxy-5-hydroxy-hept-2-enyl ester

: 868381-43-5
7-Benzyloxy-hept-1-ene-3,5-diol

Guidance literature:: With boric acid; sodium carbonate; triphenylphosphine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 50 ℃; for 1h;
DOI:10.1016/j.tetlet.2005.07.135

Reference yield:

: 184343-64-4
6-(benzyloxy)-4-hydroxyhex-1-ene

: 868381-43-5
7-Benzyloxy-hept-1-ene-3,5-diol

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / Grubbs-Hoveyda catalyst / CH₂Cl₂ / 20 °C

2: 83 percent / B(OH)3; Na₂CO₃; PPh₃ / Pd(PPh₃)4 / tetrahydrofuran / 1 h / 50 °C

With boric acid; sodium carbonate; triphenylphosphine; [1,3-bis-(2,4,6-trimethylphenyl)-2-imidazolidinylidene]dichloro(O-isopropoxyphenylmethylene)ruthenium; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tetlet.2005.07.135

Reference yield:

: 94426-72-9
2-(2-(benzyloxy)ethyl)oxirane

: 868381-43-5
7-Benzyloxy-hept-1-ene-3,5-diol

Guidance literature:: Multi-step reaction with 4 steps

1: 1) nBuLi, 2) BF₃*Et₂O / 1) THF, 2) THF

2: H₂ / Lindlar catalyst / ethanol / 760 Torr / Ambient temperature

3: tBuOOH, VO(acac)2 / toluene / -15 deg C to rt

4: nBu₄NF / tetrahydrofuran / 0.5 h / Ambient temperature

With tert.-butylhydroperoxide; n-butyllithium; bis(acetylacetonate)oxovanadium; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; hydrogen; Lindlar's catalyst; In tetrahydrofuran; ethanol; toluene;
DOI:10.1016/S0040-4039(00)92213-5