2-Amino-6-methanesulfonylbenzonitrile

Base Information

Chemical Name:2-Amino-6-methanesulfonylbenzonitrile
CAS No.:77326-37-5
Molecular Formula:C₈H₈N₂O₂S
Molecular Weight:196.23
Hs Code.:
European Community (EC) Number:851-117-6
DSSTox Substance ID:DTXSID101282933

Synonyms:2-amino-6-methanesulfonylbenzonitrile;77326-37-5;2-amino-6-methylsulfonylbenzonitrile;2-amino-6-(methylsulfonyl)benzonitrile;SCHEMBL2419183;DTXSID101282933;CDA32637;AKOS022645378;CS-0222744;EN300-112452;Z1262665669

Suppliers and Price of 2-Amino-6-methanesulfonylbenzonitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 2-Amino-6-methanesulfonylbenzonitrile

Chemical Property:

XLogP3:0.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:1
Exact Mass:196.03064868
Heavy Atom Count:13
Complexity:322

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CS(=O)(=O)C1=CC=CC(=C1C#N)N

Technology Process of 2-Amino-6-methanesulfonylbenzonitrile

There total 2 articles about 2-Amino-6-methanesulfonylbenzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 77326-38-6
2-amino-6-(methylthio)benzonitrile

: 77326-37-5
2-amino-6-(methylsulfonyl)benzonitrile

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; Heating;
DOI:10.1021/jm00138a020

Reference yield:

: 35213-00-4
2,6-dinitrobenzonitrile

: 77326-37-5
2-amino-6-(methylsulfonyl)benzonitrile

Guidance literature:: Multi-step reaction with 3 steps

1: 71 percent / dimethylformamide; H₂O / 0.17 h / 50 °C

2: 65 percent / Fe, conc. HCl / methanol / 0.25 h / Heating

3: 68 percent / m-chloroperbenzoic acid / CH₂Cl₂ / Heating

With hydrogenchloride; iron; 3-chloro-benzenecarboperoxoic acid; In methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00138a020