3,4,5,6-tetra-O-benzyl-2-deoxy-2-fluoro-scyllo-inositol-1-O-dodecylphosphonic acid

Base Information

Chemical Name:3,4,5,6-tetra-O-benzyl-2-deoxy-2-fluoro-scyllo-inositol-1-O-dodecylphosphonic acid
CAS No.:172607-64-6
Molecular Formula:C₄₆H₆₀FO₇P
Molecular Weight:774.95
Hs Code.:

Synonyms:3,4,5,6-tetra-O-benzyl-2-deoxy-2-fluoro-scyllo-inositol-1-O-dodecylphosphonic acid

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Chemical Property of 3,4,5,6-tetra-O-benzyl-2-deoxy-2-fluoro-scyllo-inositol-1-O-dodecylphosphonic acid

Chemical Property:

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Technology Process of 3,4,5,6-tetra-O-benzyl-2-deoxy-2-fluoro-scyllo-inositol-1-O-dodecylphosphonic acid

There total 6 articles about 3,4,5,6-tetra-O-benzyl-2-deoxy-2-fluoro-scyllo-inositol-1-O-dodecylphosphonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 3586-98-9
n-dodecylphosphonic acid dichloride

: 120444-22-6
(1S,2S,3R,4S,5R,6R)-2,3,4,5-Tetrakis-benzyloxy-6-fluoro-cyclohexanol

: 172607-64-6
3,4,5,6-tetra-O-benzyl-2-deoxy-2-fluoro-scyllo-inositol-1-O-dodecylphosphonic acid

Guidance literature:: With base; at 0 ℃;
DOI:10.1016/0040-4039(95)01579-5

Reference yield:

: 172722-79-1
1-O-benzoyl-3,4,5,6-tetra-O-benzyl-myo-inositol

: 172607-64-6
3,4,5,6-tetra-O-benzyl-2-deoxy-2-fluoro-scyllo-inositol-1-O-dodecylphosphonic acid

Guidance literature:: Multi-step reaction with 3 steps

1: DAST / CH₂Cl₂ / 0 °C

2: 90 percent / NaOH / H₂O

3: 75 percent / base / 0 °C

With sodium hydroxide; 4,4'-diaminostilbene-2,2'-disulfonic acid; In dichloromethane; water;
DOI:10.1016/0040-4039(95)01579-5

Reference yield:

: 24558-77-8
3,4,5,6-tetra-O-benzyl inositol

: 172607-64-6
3,4,5,6-tetra-O-benzyl-2-deoxy-2-fluoro-scyllo-inositol-1-O-dodecylphosphonic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 82 percent / base

2: DAST / CH₂Cl₂ / 0 °C

3: 90 percent / NaOH / H₂O

4: 75 percent / base / 0 °C

With sodium hydroxide; 4,4'-diaminostilbene-2,2'-disulfonic acid; In dichloromethane; water;
DOI:10.1016/0040-4039(95)01579-5