[(2,6-iPr₂C₆H₃NC(H)C(H)NC-2,6-iPr₂C₆H₃)Pd(CH₂)3C(O)OMe](B(3,5-C₆H₃(CF₃)2)4)

Base Information

• Chemical Name: [(2,6-iPr₂C₆H₃NC(H)C(H)NC-2,6-iPr₂C₆H₃)Pd(CH₂)3C(O)OMe](B(3,5-C₆H₃(CF₃)2)4)
• CAS No.: 171901-47-6
• Molecular Formula: C₃₁H₄₅N₂O₂Pd*C₃₂H₁₂BF₂₄
• Molecular Weight: 1447.35

Synonyms:[(2,6-iPr₂C₆H₃NC(H)C(H)NC-2,6-iPr₂C₆H₃)Pd(CH₂)3C(O)OMe](B(3,5-C₆H₃(CF₃)2)4)

Chemical Property of [(2,6-iPr₂C₆H₃NC(H)C(H)NC-2,6-iPr₂C₆H₃)Pd(CH₂)3C(O)OMe](B(3,5-C₆H₃(CF₃)2)4)

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Technology Process of [(2,6-iPr₂C₆H₃NC(H)C(H)NC-2,6-iPr₂C₆H₃)Pd(CH₂)3C(O)OMe](B(3,5-C₆H₃(CF₃)2)4)

There total 2 articles about [(2,6-iPr₂C₆H₃NC(H)C(H)NC-2,6-iPr₂C₆H₃)Pd(CH₂)3C(O)OMe](B(3,5-C₆H₃(CF₃)2)4) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

[(2,6-iPrC6H3NC(H)C(H)N-2,6-iPrC6H3)Pd(Me)(Cl)] + sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate (79060-88-1) + acrylic acid methyl ester (292638-85-8,9003-21-8,96-33-3) → ((((CH3)2CH)2C6H3NCH)2PdCHCH2CH3C(O)OCH3)(1+)*B(C6H3(CF3)2)4(1-)=[(((CH3)2CH)2C6H3NCH)2PdCHCH2CH3C(O)OCH3]B(C6H3(CF3)2)4 (201007-35-4) + ((((CH3)2CH)2C6H3NCH)2PdCHCH2CH3C(O)OCH3)(1+)*B(C6H3(CF3)2)4(1-)=[(((CH3)2CH)2C6H3NCH)2PdCHCH2CH3C(O)OCH3]B(C6H3(CF3)2)4 (201007-38-7) + [(2,6-iPr2C6H3NC(H)C(H)NC-2,6-iPr2C6H3)Pd(CH2)3C(O)OMe](B(3,5-C6H3(CF3)2)4) (171901-47-6)

Guidance literature:

In diethyl ether; byproducts: NaCl; inert atm.; stirring (room temp., 1-2 d); removed (NaCl), filtn. (NaCl removal), evapn. (vac.); products not sepd.; elem. anal.;

DOI:10.1021/ja964144i

Reference yield:

((((CH3)2CH)2C6H3NCH)2PdCHCH2CH3C(O)OCH3)(1+)*B(C6H3(CF3)2)4(1-)=[(((CH3)2CH)2C6H3NCH)2PdCHCH2CH3C(O)OCH3]B(C6H3(CF3)2)4 (201007-38-7) → [(2,6-iPr2C6H3NC(H)C(H)NC-2,6-iPr2C6H3)Pd(CH2)3C(O)OMe](B(3,5-C6H3(CF3)2)4) (171901-47-6)

Guidance literature:

In dichloromethane-d2; inert atm.; -20°C;

DOI:10.1021/ja964144i

upstream raw materials:

sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate

acrylic acid methyl ester

((((CH₃)2CH)2C₆H₃NCH)2PdCHCH₂CH₃C(O)OCH₃)⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=[(((CH₃)2CH)2C₆H₃NCH)2PdCHCH₂CH₃C(O)OCH₃]B(C₆H₃(CF₃)2)4

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