(R)-N-((S)-4-(dimethylamino)-3,3-dimethyl-1-morpholino-1-oxobutan-2-yl)-2,4,6-triisopropylbenzenesulfinamide

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Chemical Name:(R)-N-((S)-4-(dimethylamino)-3,3-dimethyl-1-morpholino-1-oxobutan-2-yl)-2,4,6-triisopropylbenzenesulfinamide
CAS No.:1429442-69-2
Molecular Formula:C₂₇H₄₇N₃O₃S
Molecular Weight:493.754
Hs Code.:

Synonyms:(R)-N-((S)-4-(dimethylamino)-3,3-dimethyl-1-morpholino-1-oxobutan-2-yl)-2,4,6-triisopropylbenzenesulfinamide

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Chemical Property of (R)-N-((S)-4-(dimethylamino)-3,3-dimethyl-1-morpholino-1-oxobutan-2-yl)-2,4,6-triisopropylbenzenesulfinamide

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Technology Process of (R)-N-((S)-4-(dimethylamino)-3,3-dimethyl-1-morpholino-1-oxobutan-2-yl)-2,4,6-triisopropylbenzenesulfinamide

There total 2 articles about (R)-N-((S)-4-(dimethylamino)-3,3-dimethyl-1-morpholino-1-oxobutan-2-yl)-2,4,6-triisopropylbenzenesulfinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 4394-85-8
4-morpholinecarboxaldehyde

: 1429442-63-6
(R)-N-(3-(dimethylamino)-2,2-dimethylpropylidene)-2,4,6-triisopropylbenzenesulfinamide

: 1429442-69-2
(R)-N-((S)-4-(dimethylamino)-3,3-dimethyl-1-morpholino-1-oxobutan-2-yl)-2,4,6-triisopropylbenzenesulfinamide

Guidance literature:: With lithium diisopropyl amide; In toluene; at -78 ℃; diastereoselective reaction;
DOI:10.1021/ja402647m

Reference yield:

: 15451-14-6
3-dimethylamino-2,2-dimethylpropanal

: 592507-77-2
(R)-(+)-2,4,6-triisopropylphenylsulfinamide

: 1429442-69-2
(R)-N-((S)-4-(dimethylamino)-3,3-dimethyl-1-morpholino-1-oxobutan-2-yl)-2,4,6-triisopropylbenzenesulfinamide

Guidance literature:: Multi-step reaction with 2 steps

1: titanium (IV) ethoxide / tetrahydrofuran / 16 h / 20 °C

2: lithium diisopropyl amide / toluene / -78 °C

With titanium (IV) ethoxide; lithium diisopropyl amide; In tetrahydrofuran; toluene;
DOI:10.1021/ja402647m