1-({(2R,3S)-3-[2-(8-phenyloctyl)phenyl]oxiranyl}carbonyl)-2,5-dihydropyrrole

Base Information

Chemical Name:1-({(2R,3S)-3-[2-(8-phenyloctyl)phenyl]oxiranyl}carbonyl)-2,5-dihydropyrrole
CAS No.:880175-79-1
Molecular Formula:C₂₇H₃₃NO₂
Molecular Weight:403.565
Hs Code.:

Synonyms:1-({(2R,3S)-3-[2-(8-phenyloctyl)phenyl]oxiranyl}carbonyl)-2,5-dihydropyrrole

Suppliers and Price of 1-({(2R,3S)-3-[2-(8-phenyloctyl)phenyl]oxiranyl}carbonyl)-2,5-dihydropyrrole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-({(2R,3S)-3-[2-(8-phenyloctyl)phenyl]oxiranyl}carbonyl)-2,5-dihydropyrrole

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-({(2R,3S)-3-[2-(8-phenyloctyl)phenyl]oxiranyl}carbonyl)-2,5-dihydropyrrole

There total 5 articles about 1-({(2R,3S)-3-[2-(8-phenyloctyl)phenyl]oxiranyl}carbonyl)-2,5-dihydropyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (R)-[2-(2,5-dihydro-pyrrol-1-yl)-2-oxoethyl][(2R,3S,4R)-3-methoxy-4,7,7-trimethylbicyclo[2.2.1]hept-2-yl]methylsulfonium bromide

: 96964-45-3
2-(8-phenyloctyl) benzaldehyde

: 1-({(2S,3R)-3-[2-(8-phenyloctyl)phenyl]oxiranyl}carbonyl)-2,5-dihydropyrrole

: 880175-79-1
1-({(2R,3S)-3-[2-(8-phenyloctyl)phenyl]oxiranyl}carbonyl)-2,5-dihydropyrrole

Guidance literature:: With potassium hydroxide; In methanol; at -50 ℃; for 48h; Title compound not separated from byproducts;
DOI:10.1021/ja0568345

Reference yield:

: 2-bromo-1-(2,5-dihydro-pyrrol-1-yl)-ethanone

: 880175-79-1
1-({(2R,3S)-3-[2-(8-phenyloctyl)phenyl]oxiranyl}carbonyl)-2,5-dihydropyrrole

Guidance literature:: Multi-step reaction with 2 steps

1: acetone / 24 h / 20 °C

2: KOH / methanol / 48 h / -50 °C

With potassium hydroxide; In methanol; acetone;
DOI:10.1021/ja0568345

Reference yield:

: 54636-29-2
1-chloro-7-phenylheptane

: 880175-79-1
1-({(2R,3S)-3-[2-(8-phenyloctyl)phenyl]oxiranyl}carbonyl)-2,5-dihydropyrrole

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-BuLi; 2,2,6,6-tetramethylpiperidine / tetrahydrofuran / 0.5 h / -5 - 0 °C

1.2: tetrahydrofuran / 2 h / 55 °C

1.3: 85 percent / aq. HCl / tetrahydrofuran / 2.5 h / 55 °C

2.1: KOH / methanol / 48 h / -50 °C

With 2,2,6,6-tetramethyl-piperidine; potassium hydroxide; n-butyllithium; In tetrahydrofuran; methanol;
DOI:10.1021/ja0568345