3β-hydroxy-6β-formamidomethyl-8a-phenylmethyl-trans-prehydronaphthalene

Base Information

Chemical Name:3β-hydroxy-6β-formamidomethyl-8a-phenylmethyl-trans-prehydronaphthalene
CAS No.:82911-90-8
Molecular Formula:C₁₉H₂₇NO₂
Molecular Weight:301.429
Hs Code.:

Synonyms:3β-hydroxy-6β-formamidomethyl-8a-phenylmethyl-trans-prehydronaphthalene

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Chemical Property of 3β-hydroxy-6β-formamidomethyl-8a-phenylmethyl-trans-prehydronaphthalene

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Technology Process of 3β-hydroxy-6β-formamidomethyl-8a-phenylmethyl-trans-prehydronaphthalene

There total 11 articles about 3β-hydroxy-6β-formamidomethyl-8a-phenylmethyl-trans-prehydronaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 946-33-8
2-benzylcyclohexan-1-one

: 82911-90-8
3β-hydroxy-6β-formamidomethyl-8a-phenylmethyl-trans-prehydronaphthalene

Guidance literature:: Multi-step reaction with 10 steps

1: 49 percent / potassium hydroxide / diethyl ether; ethanol / 4 h / 0 °C

2: p-toluenesulfonic acid / 3 h / 0 °C

3: 34 percent / 1.) phosphorous oxychloride, 2.) sodium acetate / 1.) methylene chloride, R_.T_. 4 h, 2.) 30 min.

4: 76 percent / hydroxylamine hydrochloride / methanol; pyridine / 0.5 h / Ambient temperature

5: 85 percent / trichloroacetonitrile / 0.5 h / Ambient temperature

6: 1.) conc. hydrochloric acid, 2.) triethylamine / 1.) THF, 1 h, 2.) benzene, 28 h

7: 76 percent / sodium borohydride / tetrahydrofuran; ethanol; H₂O / -3 °C

8: H₂ / 5percent platinum on charcoal / acetic acid / 2 h / 1551.4 Torr

9: 0.222 g / formic acid / 0.5 h

10: aq. bicarbonate / methanol / 3 h

With hydrogenchloride; potassium hydroxide; sodium tetrahydroborate; bicarbonate; hydroxylamine hydrochloride; hydrogen; sodium acetate; toluene-4-sulfonic acid; triethylamine; trichloroacetonitrile; trichlorophosphate; platinum on activated charcoal; In tetrahydrofuran; pyridine; methanol; formic acid; diethyl ether; ethanol; water; acetic acid;
DOI:10.1139/v82-151

Reference yield:

: 100-44-7
benzyl chloride

: 82911-90-8
3β-hydroxy-6β-formamidomethyl-8a-phenylmethyl-trans-prehydronaphthalene

Guidance literature:: Multi-step reaction with 11 steps

1: 55 percent / 1.) dioxane, reflux 16 h, 2.) dioxane, water, reflux, 2.5 h

2: 49 percent / potassium hydroxide / diethyl ether; ethanol / 4 h / 0 °C

3: p-toluenesulfonic acid / 3 h / 0 °C

4: 34 percent / 1.) phosphorous oxychloride, 2.) sodium acetate / 1.) methylene chloride, R_.T_. 4 h, 2.) 30 min.

5: 76 percent / hydroxylamine hydrochloride / methanol; pyridine / 0.5 h / Ambient temperature

6: 85 percent / trichloroacetonitrile / 0.5 h / Ambient temperature

7: 1.) conc. hydrochloric acid, 2.) triethylamine / 1.) THF, 1 h, 2.) benzene, 28 h

8: 76 percent / sodium borohydride / tetrahydrofuran; ethanol; H₂O / -3 °C

9: H₂ / 5percent platinum on charcoal / acetic acid / 2 h / 1551.4 Torr

10: 0.222 g / formic acid / 0.5 h

11: aq. bicarbonate / methanol / 3 h

With hydrogenchloride; potassium hydroxide; sodium tetrahydroborate; bicarbonate; hydroxylamine hydrochloride; hydrogen; sodium acetate; toluene-4-sulfonic acid; triethylamine; trichloroacetonitrile; trichlorophosphate; platinum on activated charcoal; In tetrahydrofuran; pyridine; methanol; formic acid; diethyl ether; ethanol; water; acetic acid;
DOI:10.1139/v82-151

Reference yield:

: 70043-58-2
1,2,3,5,6,7,8,8a-octahydro-3-oxo-8a-phenylmethylnaphthalene

: 82911-90-8
3β-hydroxy-6β-formamidomethyl-8a-phenylmethyl-trans-prehydronaphthalene

Guidance literature:: Multi-step reaction with 9 steps

1: p-toluenesulfonic acid / 3 h / 0 °C

2: 34 percent / 1.) phosphorous oxychloride, 2.) sodium acetate / 1.) methylene chloride, R_.T_. 4 h, 2.) 30 min.

3: 76 percent / hydroxylamine hydrochloride / methanol; pyridine / 0.5 h / Ambient temperature

4: 85 percent / trichloroacetonitrile / 0.5 h / Ambient temperature

5: 1.) conc. hydrochloric acid, 2.) triethylamine / 1.) THF, 1 h, 2.) benzene, 28 h

6: 76 percent / sodium borohydride / tetrahydrofuran; ethanol; H₂O / -3 °C

7: H₂ / 5percent platinum on charcoal / acetic acid / 2 h / 1551.4 Torr

8: 0.222 g / formic acid / 0.5 h

9: aq. bicarbonate / methanol / 3 h

With hydrogenchloride; sodium tetrahydroborate; bicarbonate; hydroxylamine hydrochloride; hydrogen; sodium acetate; toluene-4-sulfonic acid; triethylamine; trichloroacetonitrile; trichlorophosphate; platinum on activated charcoal; In tetrahydrofuran; pyridine; methanol; formic acid; ethanol; water; acetic acid;
DOI:10.1139/v82-151