Thiobenzoic acid S-((1S,4R)-7,7-dimethyl-2-oxo-bicyclo[2.2.1]hept-1-ylmethyl) ester

Base Information

Chemical Name:Thiobenzoic acid S-((1S,4R)-7,7-dimethyl-2-oxo-bicyclo[2.2.1]hept-1-ylmethyl) ester
CAS No.:186391-64-0
Molecular Formula:C₁₇H₂₀O₂S
Molecular Weight:288.411
Hs Code.:

Synonyms:Thiobenzoic acid S-((1S,4R)-7,7-dimethyl-2-oxo-bicyclo[2.2.1]hept-1-ylmethyl) ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Thiobenzoic acid S-((1S,4R)-7,7-dimethyl-2-oxo-bicyclo[2.2.1]hept-1-ylmethyl) ester

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Technology Process of Thiobenzoic acid S-((1S,4R)-7,7-dimethyl-2-oxo-bicyclo[2.2.1]hept-1-ylmethyl) ester

There total 1 articles about Thiobenzoic acid S-((1S,4R)-7,7-dimethyl-2-oxo-bicyclo[2.2.1]hept-1-ylmethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 54984-43-9,77026-99-4
(1S,4R)-camphor-10-thiol

: 98-88-4
benzoyl chloride

: 186391-64-0
Thiobenzoic acid S-((1S,4R)-7,7-dimethyl-2-oxo-bicyclo[2.2.1]hept-1-ylmethyl) ester

Guidance literature:: With dmap; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1016/S0957-4166(96)00463-6

Reference yield: 84.0%

: 186391-64-0
Thiobenzoic acid S-((1S,4R)-7,7-dimethyl-2-oxo-bicyclo[2.2.1]hept-1-ylmethyl) ester

: 186391-65-1
Dithiobenzoic acid (1R,4R)-7,7-dimethyl-2-thioxo-bicyclo[2.2.1]hept-1-ylmethyl ester

Guidance literature:: With Lawessons reagent; In toluene; for 2.5h; Heating;
DOI:10.1016/S0957-4166(96)00463-6

Reference yield:

: 186391-64-0
Thiobenzoic acid S-((1S,4R)-7,7-dimethyl-2-oxo-bicyclo[2.2.1]hept-1-ylmethyl) ester

: (1R,4R)-1-Mercaptomethyl-7,7-dimethyl-bicyclo[2.2.1]heptane-2-thiol

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / Lawesson's reagent / toluene / 2.5 h / Heating

2: LiAlH₄ / diethyl ether / 0.5 h / Ambient temperature

With Lawessons reagent; lithium aluminium tetrahydride; In diethyl ether; toluene;
DOI:10.1016/S0957-4166(96)00463-6