(3E,7E)-2-Benzenesulfonyl-2-[(2E,6E)-8-(5-methoxy-2-methoxycarbonyloxy-phenyl)-2,6-dimethyl-octa-2,6-dienyl]-4,8,12-trimethyl-trideca-3,7,11-trienoic acid methyl ester

Base Information

Chemical Name:(3E,7E)-2-Benzenesulfonyl-2-[(2E,6E)-8-(5-methoxy-2-methoxycarbonyloxy-phenyl)-2,6-dimethyl-octa-2,6-dienyl]-4,8,12-trimethyl-trideca-3,7,11-trienoic acid methyl ester
CAS No.:191401-75-9
Molecular Formula:C₄₂H₅₆O₈S
Molecular Weight:720.968
Hs Code.:

(3E,7E)-2-Benzenesulfonyl-2-[(2E,6E)-8-(5-methoxy-2-methoxycarbonyloxy-phenyl)-2,6-dimethyl-octa-2,6-dienyl]-4,8,12-trimethyl-trideca-3,7,11-trienoic acid methyl ester

Synonyms:(3E,7E)-2-Benzenesulfonyl-2-[(2E,6E)-8-(5-methoxy-2-methoxycarbonyloxy-phenyl)-2,6-dimethyl-octa-2,6-dienyl]-4,8,12-trimethyl-trideca-3,7,11-trienoic acid methyl ester

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Chemical Property of (3E,7E)-2-Benzenesulfonyl-2-[(2E,6E)-8-(5-methoxy-2-methoxycarbonyloxy-phenyl)-2,6-dimethyl-octa-2,6-dienyl]-4,8,12-trimethyl-trideca-3,7,11-trienoic acid methyl ester

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Technology Process of (3E,7E)-2-Benzenesulfonyl-2-[(2E,6E)-8-(5-methoxy-2-methoxycarbonyloxy-phenyl)-2,6-dimethyl-octa-2,6-dienyl]-4,8,12-trimethyl-trideca-3,7,11-trienoic acid methyl ester

There total 9 articles about (3E,7E)-2-Benzenesulfonyl-2-[(2E,6E)-8-(5-methoxy-2-methoxycarbonyloxy-phenyl)-2,6-dimethyl-octa-2,6-dienyl]-4,8,12-trimethyl-trideca-3,7,11-trienoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 159108-84-6
(3E,7E)-methyl 2-benzenesulfonyl-4,8,12-trimethyltrideca-3,7,11-trienoate

: 191401-67-9
Carbonic acid 4-methoxy-2-((E)-6-methoxycarbonyloxy-3,7-dimethyl-octa-2,7-dienyl)-phenyl ester methyl ester

: 191401-75-9
(3E,7E)-2-Benzenesulfonyl-2-[(2E,6E)-8-(5-methoxy-2-methoxycarbonyloxy-phenyl)-2,6-dimethyl-octa-2,6-dienyl]-4,8,12-trimethyl-trideca-3,7,11-trienoic acid methyl ester

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 25 ℃;

Reference yield:

: 6138-90-5
trans-geranyl bromide

: 191401-75-9
(3E,7E)-2-Benzenesulfonyl-2-[(2E,6E)-8-(5-methoxy-2-methoxycarbonyloxy-phenyl)-2,6-dimethyl-octa-2,6-dienyl]-4,8,12-trimethyl-trideca-3,7,11-trienoic acid methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 82 percent / Na / diethyl ether / 48 h / 36 °C

2: 65 percent / 3-chloroperoxybenzoic acid / CH₂Cl₂ / 0.25 h / -5 - 0 °C

3: 95 percent / Al(Oi-Pr)3 / toluene / 110 °C

4: 94 percent / diethylaniline, pyridine / benzene / 4 h / Ambient temperature

5: 90 percent / Pd(PPh₃)4 / tetrahydrofuran / 25 °C

With pyridine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium; aluminum isopropoxide; 3-chloro-benzenecarboperoxoic acid; N,N-diethylaniline; In tetrahydrofuran; diethyl ether; dichloromethane; toluene; benzene;

Reference yield:

: 106-28-5
Farnesol

: 191401-75-9
(3E,7E)-2-Benzenesulfonyl-2-[(2E,6E)-8-(5-methoxy-2-methoxycarbonyloxy-phenyl)-2,6-dimethyl-octa-2,6-dienyl]-4,8,12-trimethyl-trideca-3,7,11-trienoic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / PBr₃ / diethyl ether / -20 °C

2: 80 percent / dimethylformamide / 20 °C

3: 90 percent / t-BuOK / -5 - 0 °C

4: 90 percent / Pd(PPh₃)4 / tetrahydrofuran / 25 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium tert-butylate; phosphorus tribromide; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide;