2-(9H-fluoren-9-ylmethoxycarbonylamino)-pentanedioic acid 5-[bis-(4-fluoro-phenyl)-pentafluorophenyl-methyl] ester

Base Information

Chemical Name:2-(9H-fluoren-9-ylmethoxycarbonylamino)-pentanedioic acid 5-[bis-(4-fluoro-phenyl)-pentafluorophenyl-methyl] ester
CAS No.:241823-99-4
Molecular Formula:C₃₉H₂₆F₇NO₆
Molecular Weight:737.627
Hs Code.:

2-(9<i>H</i>-fluoren-9-ylmethoxycarbonylamino)-pentanedioic acid 5-[bis-(4-fluoro-phenyl)-pentafluorophenyl-methyl] ester

Synonyms:2-(9H-fluoren-9-ylmethoxycarbonylamino)-pentanedioic acid 5-[bis-(4-fluoro-phenyl)-pentafluorophenyl-methyl] ester

Suppliers and Price of 2-(9H-fluoren-9-ylmethoxycarbonylamino)-pentanedioic acid 5-[bis-(4-fluoro-phenyl)-pentafluorophenyl-methyl] ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(9H-fluoren-9-ylmethoxycarbonylamino)-pentanedioic acid 5-[bis-(4-fluoro-phenyl)-pentafluorophenyl-methyl] ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 2-(9H-fluoren-9-ylmethoxycarbonylamino)-pentanedioic acid 5-[bis-(4-fluoro-phenyl)-pentafluorophenyl-methyl] ester

There total 6 articles about 2-(9H-fluoren-9-ylmethoxycarbonylamino)-pentanedioic acid 5-[bis-(4-fluoro-phenyl)-pentafluorophenyl-methyl] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 241823-97-2
2-(9H-fluoren-9-ylmethoxycarbonylamino)-pentanedioic acid 1-allyl ester 5-[bis-(4-fluoro-phenyl)-pentafluorophenyl-methyl] ester

: 241823-99-4
2-(9H-fluoren-9-ylmethoxycarbonylamino)-pentanedioic acid 5-[bis-(4-fluoro-phenyl)-pentafluorophenyl-methyl] ester

Guidance literature:: With N-methylaniline; tetrakis(triphenylphosphine) palladium⁽⁰⁾;

Reference yield:

: 344-04-7
bromopentafluorobenzene

: 241823-99-4
2-(9H-fluoren-9-ylmethoxycarbonylamino)-pentanedioic acid 5-[bis-(4-fluoro-phenyl)-pentafluorophenyl-methyl] ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: Mg / diethyl ether

1.2: 94 percent / diethyl ether / 3 h / Heating

2.1: 100 percent / SOCl₂ / 0.17 h / 20 °C

3.1: 84 percent / DIPEA / CH₂Cl₂ / 14 h / 20 °C

4.1: 82 percent / PhNHMe / Pd(PPh₃)4

With thionyl chloride; magnesium; N-ethyl-N,N-diisopropylamine; N-methylaniline; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In diethyl ether; dichloromethane; 1.1: Metallation / 1.2: Grignard reaction / 2.1: Substitution / 3.1: Alkylation / 4.1: Deallylation;

Reference yield:

: 345-92-6
4,4'-Difluorobenzophenone

: 241823-99-4
2-(9H-fluoren-9-ylmethoxycarbonylamino)-pentanedioic acid 5-[bis-(4-fluoro-phenyl)-pentafluorophenyl-methyl] ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: Mg / diethyl ether

1.2: 94 percent / diethyl ether / 3 h / Heating

2.1: 100 percent / SOCl₂ / 0.17 h / 20 °C

3.1: 84 percent / DIPEA / CH₂Cl₂ / 14 h / 20 °C

4.1: 82 percent / PhNHMe / Pd(PPh₃)4

With thionyl chloride; magnesium; N-ethyl-N,N-diisopropylamine; N-methylaniline; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In diethyl ether; dichloromethane; 1.1: Metallation / 1.2: Grignard reaction / 2.1: Substitution / 3.1: Alkylation / 4.1: Deallylation;