tert-butyl O-[( 1H-benzotriazol-1-yloxy)methyl]-N-(tert-butoxycarbonyl)-D-tyrosinate

Base Information

Chemical Name:tert-butyl O-[( 1H-benzotriazol-1-yloxy)methyl]-N-(tert-butoxycarbonyl)-D-tyrosinate
CAS No.:1417187-37-1
Molecular Formula:C₂₅H₃₂N₄O₆
Molecular Weight:484.552
Hs Code.:

Synonyms:tert-butyl O-[( 1H-benzotriazol-1-yloxy)methyl]-N-(tert-butoxycarbonyl)-D-tyrosinate

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Chemical Property of tert-butyl O-[( 1H-benzotriazol-1-yloxy)methyl]-N-(tert-butoxycarbonyl)-D-tyrosinate

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Technology Process of tert-butyl O-[( 1H-benzotriazol-1-yloxy)methyl]-N-(tert-butoxycarbonyl)-D-tyrosinate

There total 4 articles about tert-butyl O-[( 1H-benzotriazol-1-yloxy)methyl]-N-(tert-butoxycarbonyl)-D-tyrosinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1417188-25-0
tert-butyl N-(tert-butoxycarbonyl)-O-[(methylsulfanyl)methyl]-D-tyrosinate

: 1417187-37-1
tert-butyl O-[( 1H-benzotriazol-1-yloxy)methyl]-N-(tert-butoxycarbonyl)-D-tyrosinate

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-chloro-succinimide / dichloromethane / 0.17 h / 20 °C

1.2: 20 °C

2.1: dmap / dichloromethane; N,N-dimethyl-formamide / 0.5 h / 20 °C

With dmap; N-chloro-succinimide; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1417187-37-1
tert-butyl O-[( 1H-benzotriazol-1-yloxy)methyl]-N-(tert-butoxycarbonyl)-D-tyrosinate

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / dichloromethane; N,N-dimethyl-formamide / 2 h / 20 °C

2.1: sodium iodide; potassium tert-butylate / N,N-dimethyl-formamide; tetrahydrofuran / 3 h / 20 °C / Cooling with ice

3.1: N-chloro-succinimide / dichloromethane / 0.17 h / 20 °C

3.2: 20 °C

4.1: dmap / dichloromethane; N,N-dimethyl-formamide / 0.5 h / 20 °C

With dmap; N-chloro-succinimide; potassium tert-butylate; triethylamine; sodium iodide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1414025-67-4
(R)-tert-butyl 2-(tert-butoxycarbonylamino) -3-(4-hydroxyphenyl)propanoate

: 1417187-37-1
tert-butyl O-[( 1H-benzotriazol-1-yloxy)methyl]-N-(tert-butoxycarbonyl)-D-tyrosinate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium iodide; potassium tert-butylate / N,N-dimethyl-formamide; tetrahydrofuran / 3 h / 20 °C / Cooling with ice

2.1: N-chloro-succinimide / dichloromethane / 0.17 h / 20 °C

2.2: 20 °C

3.1: dmap / dichloromethane; N,N-dimethyl-formamide / 0.5 h / 20 °C

With dmap; N-chloro-succinimide; potassium tert-butylate; sodium iodide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;