(2S,3S)-ethyl N-[tert-butyl-(S)-sulfinyl]-3-p-nitrophenylaziridine-2-carboxylate

Base Information

• Chemical Name: (2S,3S)-ethyl N-[tert-butyl-(S)-sulfinyl]-3-p-nitrophenylaziridine-2-carboxylate
• CAS No.: 1316220-54-8
• Molecular Formula: C₁₅H₂₀N₂O₅S
• Molecular Weight: 340.4

Synonyms:(2S,3S)-ethyl N-[tert-butyl-(S)-sulfinyl]-3-p-nitrophenylaziridine-2-carboxylate

Chemical Property of (2S,3S)-ethyl N-[tert-butyl-(S)-sulfinyl]-3-p-nitrophenylaziridine-2-carboxylate

Chemical Property:

Purity/Quality:

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Technology Process of (2S,3S)-ethyl N-[tert-butyl-(S)-sulfinyl]-3-p-nitrophenylaziridine-2-carboxylate

There total 1 articles about (2S,3S)-ethyl N-[tert-butyl-(S)-sulfinyl]-3-p-nitrophenylaziridine-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

(S)-N-(4-nitrobenzylidene)-2-methylpropane-2-sulfinamide + ethyl bromoacetate (105-36-2) → (2S,3S)-ethyl N-[tert-butyl-(S)-sulfinyl]-3-p-nitrophenylaziridine-2-carboxylate (1316220-54-8) + ethyl N-[tert-butyl-(S)-sulfinyl]-3-p-nitrophenylaziridine-2-carboxylate

Guidance literature:

ethyl bromoacetate; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 0.5h; Inert atmosphere;

(S)-N-(4-nitrobenzylidene)-2-methylpropane-2-sulfinamide; In tetrahydrofuran; at -78 ℃; optical yield given as %de; diastereoselective reaction;

DOI:10.1039/c1ob05561e

upstream raw materials:

ethyl bromoacetate

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