1-benzylpiperidine-¹⁵N

Base Information

Chemical Name:1-benzylpiperidine-¹⁵N
CAS No.:1438854-08-0
Molecular Formula:C₁₂H₁₇N
Molecular Weight:176.267
Hs Code.:

Synonyms:1-benzylpiperidine-¹⁵N

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-benzylpiperidine-¹⁵N

Chemical Property:

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Technology Process of 1-benzylpiperidine-¹⁵N

There total 3 articles about 1-benzylpiperidine-¹⁵N which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1438854-07-9
1-benzoylpiperidine-¹⁵N

: 1438854-08-0
1-benzylpiperidine-¹⁵N

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at 0 ℃; for 18h; Inert atmosphere;
DOI:10.1021/ja403076u

Reference yield:

: 31656-62-9
¹⁵N-benzamide

: 1438854-08-0
1-benzylpiperidine-¹⁵N

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate / toluene / 18 h / Reflux; Inert atmosphere

2: lithium aluminium tetrahydride / diethyl ether / 18 h / 0 °C / Inert atmosphere

With lithium aluminium tetrahydride; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; sodium hydroxide; In diethyl ether; toluene;
DOI:10.1021/ja403076u

Reference yield:

: 98-88-4
benzoyl chloride

: 1438854-08-0
1-benzylpiperidine-¹⁵N

Guidance literature:: Multi-step reaction with 3 steps

1: ammonium-¹⁵N hydrochloride; sodium hydroxide / water; diethyl ether / 0.25 h / 0 °C / Inert atmosphere

2: sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate / toluene / 18 h / Reflux; Inert atmosphere

3: lithium aluminium tetrahydride / diethyl ether / 18 h / 0 °C / Inert atmosphere

With lithium aluminium tetrahydride; ammonium-¹⁵N hydrochloride; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; sodium hydroxide; In diethyl ether; water; toluene;
DOI:10.1021/ja403076u