2-acetoxy-2-(2,7-dimethoxy-1-naphthyl)-N-(2'-methoxyphenyl)-3-oxobutanamide

Base Information

• Chemical Name: 2-acetoxy-2-(2,7-dimethoxy-1-naphthyl)-N-(2'-methoxyphenyl)-3-oxobutanamide
• CAS No.: 1092963-80-8
• Molecular Formula: C₂₅H₂₅NO₇
• Molecular Weight: 451.476

Synonyms:2-acetoxy-2-(2,7-dimethoxy-1-naphthyl)-N-(2'-methoxyphenyl)-3-oxobutanamide

Chemical Property of 2-acetoxy-2-(2,7-dimethoxy-1-naphthyl)-N-(2'-methoxyphenyl)-3-oxobutanamide

Chemical Property:

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Technology Process of 2-acetoxy-2-(2,7-dimethoxy-1-naphthyl)-N-(2'-methoxyphenyl)-3-oxobutanamide

There total 1 articles about 2-acetoxy-2-(2,7-dimethoxy-1-naphthyl)-N-(2'-methoxyphenyl)-3-oxobutanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

2'-methoxyacetoacetanilide (92-15-9) + 2,7-Dimethoxynaphthalene (3469-26-9) + manganese triacetate (638-38-0,993-02-2,2180-18-9,15411-95-7,22981-23-3,27004-39-3) → 1-acetyl-1-hydroxy-8-methoxy-3-(2'-methoxyphenyl)-1H-benzo[e]indol-2(3H)-one (1092964-03-8) + C24H21NO6 + 2-acetoxy-2-(2,7-dimethoxy-1-naphthyl)-N-(2'-methoxyphenyl)-3-oxobutanamide (1092963-80-8)

Guidance literature:

With acetic acid; at 70 ℃; for 0.0333333h;

DOI:10.1055/s-2008-1067206

Reference yield: 81.0%

2-acetoxy-2-(2,7-dimethoxy-1-naphthyl)-N-(2'-methoxyphenyl)-3-oxobutanamide (1092963-80-8) → 5-chloro-1-(2-methoxyphenylcarbamoyl)-8-methoxy-2-methylnaphtho[2,1-b]furan (1134953-11-9)

Guidance literature:

With hydrogenchloride; In water; acetic acid; at 20 ℃; for 5h;

DOI:10.3987/COM-08-11515

upstream raw materials:

2'-methoxyacetoacetanilide

2,7-Dimethoxynaphthalene

manganese triacetate

Downstream raw materials:

5-chloro-1-(2-methoxyphenylcarbamoyl)-8-methoxy-2-methylnaphtho[2,1-b]furan

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