6-hexanoic acid N-hydroxysuccinimide ester

Base Information

Chemical Name:6-hexanoic acid N-hydroxysuccinimide ester
CAS No.:156272-90-1
Molecular Formula:C₂₉H₃₀N₂O₆
Molecular Weight:502.567
Hs Code.:

6-<N-carbobenzoxy-N-(2-naphthylmethyl)amino>hexanoic acid N-hydroxysuccinimide ester

Synonyms:6-hexanoic acid N-hydroxysuccinimide ester

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Chemical Property of 6-hexanoic acid N-hydroxysuccinimide ester

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Technology Process of 6-hexanoic acid N-hydroxysuccinimide ester

There total 5 articles about 6-hexanoic acid N-hydroxysuccinimide ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 6066-82-6
1-hydroxy-pyrrolidine-2,5-dione

: 156272-89-8
6-hexanoic acid

: 156272-90-1
6-hexanoic acid N-hydroxysuccinimide ester

Guidance literature:: With dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1021/jm00040a018

Reference yield:

: 66-99-9
β-naphthaldehyde

: 156272-90-1
6-hexanoic acid N-hydroxysuccinimide ester

Guidance literature:: Multi-step reaction with 4 steps

1: toluene / 18 h / Heating

2: sodium borohydride / ethanol / 8 h

3: 97 percent / NaHCO₃ / H₂O / 6 h / 0 °C

4: 70 percent / dicyclohexylcarbodiimide / CH₂Cl₂

With sodium tetrahydroborate; sodium hydrogencarbonate; dicyclohexyl-carbodiimide; In ethanol; dichloromethane; water; toluene;
DOI:10.1021/jm00040a018

Reference yield:

: 6-{[1-Naphthalen-2-yl-meth-(E)-ylidene]-amino}-hexanoic acid

: 156272-90-1
6-hexanoic acid N-hydroxysuccinimide ester

Guidance literature:: Multi-step reaction with 3 steps

1: sodium borohydride / ethanol / 8 h

2: 97 percent / NaHCO₃ / H₂O / 6 h / 0 °C

3: 70 percent / dicyclohexylcarbodiimide / CH₂Cl₂

With sodium tetrahydroborate; sodium hydrogencarbonate; dicyclohexyl-carbodiimide; In ethanol; dichloromethane; water;
DOI:10.1021/jm00040a018