N-(6,6-difluoro-4-iodo-3,3-dimethyl-6-(phenylthio)-hexyl)-benzenesulfonamide

Base Information

Chemical Name:N-(6,6-difluoro-4-iodo-3,3-dimethyl-6-(phenylthio)-hexyl)-benzenesulfonamide
CAS No.:1268994-71-3
Molecular Formula:C₂₀H₂₄F₂INO₂S₂
Molecular Weight:539.449
Hs Code.:

Synonyms:N-(6,6-difluoro-4-iodo-3,3-dimethyl-6-(phenylthio)-hexyl)-benzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(6,6-difluoro-4-iodo-3,3-dimethyl-6-(phenylthio)-hexyl)-benzenesulfonamide

Chemical Property:

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Technology Process of N-(6,6-difluoro-4-iodo-3,3-dimethyl-6-(phenylthio)-hexyl)-benzenesulfonamide

There total 6 articles about N-(6,6-difluoro-4-iodo-3,3-dimethyl-6-(phenylthio)-hexyl)-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1268994-50-8
N-phenylsulfonyl-3,3-dimethyl-pent-4-en-1-amine

: 272788-38-2
iododifluoromethyl phenyl thioether

: 1268994-71-3
N-(6,6-difluoro-4-iodo-3,3-dimethyl-6-(phenylthio)-hexyl)-benzenesulfonamide

Guidance literature:: With sodium dithionite; sodium hydroxide; In water; acetonitrile; at 20 ℃; for 5h;
DOI:10.1016/j.tet.2010.11.090

Reference yield:

: 70184-93-9
3,3-dimethyl-pent-4-enoic acid amide

: 1268994-71-3
N-(6,6-difluoro-4-iodo-3,3-dimethyl-6-(phenylthio)-hexyl)-benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / diethyl ether / 20 °C / Inert atmosphere; Cooling with ice

2: pyridine; sodium hydroxide / 3 h / 20 °C / pH 11

3: sodium dithionite; sodium hydroxide / water; acetonitrile / 5 h / 20 °C

With pyridine; lithium aluminium tetrahydride; sodium dithionite; sodium hydroxide; In diethyl ether; water; acetonitrile;
DOI:10.1016/j.tet.2010.11.090

Reference yield:

: 7796-73-8
3,3-dimethylpent-4-enoic acid

: 1268994-71-3
N-(6,6-difluoro-4-iodo-3,3-dimethyl-6-(phenylthio)-hexyl)-benzenesulfonamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: thionyl chloride / dichloromethane / 0.5 h / Cooling with ice

1.2: 5 h / Reflux

2.1: ammonia / water / 10 h / 20 °C

3.1: lithium aluminium tetrahydride / diethyl ether / 20 °C / Inert atmosphere; Cooling with ice

4.1: pyridine; sodium hydroxide / 3 h / 20 °C / pH 11

5.1: sodium dithionite; sodium hydroxide / water; acetonitrile / 5 h / 20 °C

With pyridine; lithium aluminium tetrahydride; thionyl chloride; sodium dithionite; ammonia; sodium hydroxide; In diethyl ether; dichloromethane; water; acetonitrile;
DOI:10.1016/j.tet.2010.11.090