methyl (2E)-3-(3,4-dimethoxyphenyl)-2-(6-methoxy-3-oxoprop-1-en-2-yl-2,3-dimethoxyphenyl)prop-2-enoate

Base Information

• Chemical Name: methyl (2E)-3-(3,4-dimethoxyphenyl)-2-(6-methoxy-3-oxoprop-1-en-2-yl-2,3-dimethoxyphenyl)prop-2-enoate
• CAS No.: 1065559-67-2
• Molecular Formula: C₂₃H₂₄O₈
• Molecular Weight: 428.439
• Mol file: 1065559-67-2.mol

Synonyms:methyl (2E)-3-(3,4-dimethoxyphenyl)-2-(6-methoxy-3-oxoprop-1-en-2-yl-2,3-dimethoxyphenyl)prop-2-enoate

Chemical Property of methyl (2E)-3-(3,4-dimethoxyphenyl)-2-(6-methoxy-3-oxoprop-1-en-2-yl-2,3-dimethoxyphenyl)prop-2-enoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of methyl (2E)-3-(3,4-dimethoxyphenyl)-2-(6-methoxy-3-oxoprop-1-en-2-yl-2,3-dimethoxyphenyl)prop-2-enoate

There total 1 articles about methyl (2E)-3-(3,4-dimethoxyphenyl)-2-(6-methoxy-3-oxoprop-1-en-2-yl-2,3-dimethoxyphenyl)prop-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

malonic acid (141-82-2) + methyl (2E)-3-(3,4-dimethoxyphenyl)-2-(6-formyl-2,3-dimethoxyphenyl)prop-2-enoate (1065559-63-8) → methyl (2E)-3-(3,4-dimethoxyphenyl)-2-(6-methoxy-3-oxoprop-1-en-2-yl-2,3-dimethoxyphenyl)prop-2-enoate (1065559-67-2)

Guidance literature:

With piperidine; In pyridine; for 10h; Reflux;

DOI:10.1016/j.bmcl.2008.06.063

Reference yield: 75.0%

methyl (2E)-3-(3,4-dimethoxyphenyl)-2-(6-methoxy-3-oxoprop-1-en-2-yl-2,3-dimethoxyphenyl)prop-2-enoate (1065559-67-2) → (E)-3-(2,3,6-trihydroxy-10-oxo-9b,10-dihydro-4bH-benzo[b]indeno[2,1-d]furan-9-yl) acrylic acid + (2E)-2-{6-[(E)-2-carboxyvinyl]-2,3-dihydroxyphenyl}-3-(3,4-dihydroxyphenyl) propenoic acid (1065559-56-9)

Guidance literature:

With boron tribromide; In dichloromethane; at 20 ℃; for 12h;

DOI:10.1016/j.bmcl.2008.06.063

Reference yield: 60.0%

methyl (2E)-3-(3,4-dimethoxyphenyl)-2-(6-methoxy-3-oxoprop-1-en-2-yl-2,3-dimethoxyphenyl)prop-2-enoate (1065559-67-2) → C19H16O8 (1065559-69-4)

Guidance literature:

With boron tribromide; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1016/j.bmcl.2008.06.063

upstream raw materials:

malonic acid

methyl (2E)-3-(3,4-dimethoxyphenyl)-2-(6-formyl-2,3-dimethoxyphenyl)prop-2-enoate

Downstream raw materials:

C₁₉H₁₆O₈

(2E)-2-{6-[(E)-2-carboxyvinyl]-2,3-dihydroxyphenyl}-3-(3,4-dihydroxyphenyl) propenoic acid