Technology Process of 2,3-di-O-benzyl-2-C-methyl-L-glycerylaldehyde
There total 11 articles about 2,3-di-O-benzyl-2-C-methyl-L-glycerylaldehyde which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium periodate;
In
methanol; water;
for 0.666667h;
Ambient temperature;
DOI:10.1246/bcsj.55.933
- Guidance literature:
-
Multi-step reaction with 9 steps
1: 95 percent / pyridine / 1 h / Ambient temperature
2: 96 percent / acetic acid / H2O / 2 h / Heating
3: 83 percent / sodium periodate / methanol; H2O / 0.5 h / Ambient temperature
4: 92 percent / NaBH4 / methanol; H2O / 3 h / Ambient temperature
5: 74 percent / CH3ONa / methanol / 3 h / Ambient temperature
6: 70 percent / H2SO4 / 48 h / Ambient temperature
7: 68 percent / NaH / dimethylformamide / 12 h
8: 84 percent / acetic acid / H2O / 72 h / Ambient temperature
9: 95 percent / sodium periodate / methanol; H2O / 0.67 h / Ambient temperature
With
pyridine; sodium tetrahydroborate; sodium periodate; sulfuric acid; sodium methylate; sodium hydride; acetic acid;
In
methanol; water; N,N-dimethyl-formamide;
DOI:10.1246/bcsj.55.933
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 68 percent / NaH / dimethylformamide / 12 h
2: 84 percent / acetic acid / H2O / 72 h / Ambient temperature
3: 95 percent / sodium periodate / methanol; H2O / 0.67 h / Ambient temperature
With
sodium periodate; sodium hydride; acetic acid;
In
methanol; water; N,N-dimethyl-formamide;
DOI:10.1246/bcsj.55.933
