1,6-DI-(N-Carbazolyl)-2,4-hexadiyne

Base Information

Chemical Name:1,6-DI-(N-Carbazolyl)-2,4-hexadiyne
CAS No.:65461-62-3
Molecular Formula:C₃₀H₂₀N₂
Molecular Weight:408.502
Hs Code.:2933990090
DSSTox Substance ID:DTXSID30598920
Nikkaji Number:J497.593F
Wikidata:Q82494734

Synonyms:65461-62-3;1,6-Bis(9H-carbazole-9-yl)2,4-hexadiyne;1,6-DI-(N-CARBAZOLYL)-2,4-HEXADIYNE;1,6-Di(9H-carbazol-9-yl)hexa-2,4-diyne;9-(6-carbazol-9-ylhexa-2,4-diynyl)carbazole;SCHEMBL8335552;DTXSID30598920;1,6-di(N-carbazolyl)-2,4-hexadiyne;G71525;9,9'-(Hexa-2,4-diyne-1,6-diyl)di(9H-carbazole);9-[6-(carbazol-9-yl)hexa-2,4-diyn-1-yl]carbazole

Suppliers and Price of 1,6-DI-(N-Carbazolyl)-2,4-hexadiyne

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1,6-DI-(N-CARBAZOLYL)-2,4-HEXADIYNE 95.00%
5MG
$ 500.14

Total 5 raw suppliers

Chemical Property of 1,6-DI-(N-Carbazolyl)-2,4-hexadiyne

Chemical Property:

PSA：9.86000
LogP:6.60940
XLogP3:7.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:3
Exact Mass:408.162648646
Heavy Atom Count:32
Complexity:692

Purity/Quality:

98%+ ^*data from raw suppliers

1,6-DI-(N-CARBAZOLYL)-2,4-HEXADIYNE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C3=CC=CC=C3N2CC#CC#CCN4C5=CC=CC=C5C6=CC=CC=C64

Technology Process of 1,6-DI-(N-Carbazolyl)-2,4-hexadiyne

There total 4 articles about 1,6-DI-(N-Carbazolyl)-2,4-hexadiyne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 4282-77-3
9-(prop-2-yn-1-yl)-9H-carbazole

: 65461-62-3
1,6-di(N-carbazolyl)-2,4-hexadiyne

Guidance literature:: With oxygen; copper(l) chloride; In dimethyl sulfoxide; at 90 ℃; for 4h;
DOI:10.1039/c4ra11571f

Reference yield:

green-gold: green-gold

: 4282-77-3
9-(prop-2-yn-1-yl)-9H-carbazole

: 65461-62-3
1,6-di(N-carbazolyl)-2,4-hexadiyne

Guidance literature:: With hydrogenchloride; copper(I) chloride; In 1,4-dioxane;

Reference yield:

: 86-74-8,105184-46-1,97960-57-1
9H-carbazole

: 65461-62-3
1,6-di(N-carbazolyl)-2,4-hexadiyne

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / N,N-dimethyl-formamide / 0.25 h / 0 °C

1.2: 6 h / 20 °C

2.1: copper(l) chloride; oxygen / dimethyl sulfoxide / 4 h / 90 °C

With oxygen; copper(l) chloride; potassium hydroxide; In dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1039/c4ra11571f