2-Chloro-4-hydroxy-3-methoxybenzenemethanol

Base Information

Chemical Name:2-Chloro-4-hydroxy-3-methoxybenzenemethanol
CAS No.:110038-86-3
Molecular Formula:C₈H₉ClO₃
Molecular Weight:188.611
Hs Code.:

Synonyms:2-Chloro-4-hydroxy-3-methoxybenzenemethanol

Suppliers and Price of 2-Chloro-4-hydroxy-3-methoxybenzenemethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Chloro-4-hydroxy-3-methoxybenzenemethanol

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Technology Process of 2-Chloro-4-hydroxy-3-methoxybenzenemethanol

There total 3 articles about 2-Chloro-4-hydroxy-3-methoxybenzenemethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 82668-20-0
2-Chlorovanillin

: 110038-86-3
2-Chloro-4-hydroxy-3-methoxybenzenemethanol

Guidance literature:: With sodium tetrahydroborate; In isopropyl alcohol; at 70 ℃; for 1h;
DOI:10.1002/jhet.5570230641

Reference yield:

: 881-68-5
vanillin acetate

: 110038-86-3
2-Chloro-4-hydroxy-3-methoxybenzenemethanol

Guidance literature:: Multi-step reaction with 4 steps

1: 81 percent / fuming HNO₃ / -20 °C

2: 79 percent / 1.) FeSO₄, aq. HCl, 2.) 15 N ammonium hydroxide; / 90 °C

3: 1.) aq. HCl, NaNO₂, 2.) Cu₂Cl₂; / 1.) water, 0 deg C, 2.) temperature below 5 deg C, 3.) heating on steam bath, 1 h;

4: 89 percent / NaBH₄ / propan-2-ol / 1 h / 70 °C

With copper(I) chloride; hydrogenchloride; ammonium hydroxide; sodium tetrahydroborate; nitric acid; iron(II) sulfate; sodium nitrite; In isopropyl alcohol;
DOI:10.1002/jhet.5570230641

Reference yield:

: 89984-23-6
2-amino-4-hydroxy-3-methoxy-benzaldehyde

: 110038-86-3
2-Chloro-4-hydroxy-3-methoxybenzenemethanol

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) aq. HCl, NaNO₂, 2.) Cu₂Cl₂; / 1.) water, 0 deg C, 2.) temperature below 5 deg C, 3.) heating on steam bath, 1 h;

2: 89 percent / NaBH₄ / propan-2-ol / 1 h / 70 °C

With copper(I) chloride; hydrogenchloride; sodium tetrahydroborate; sodium nitrite; In isopropyl alcohol;
DOI:10.1002/jhet.5570230641