C₃₈H₄₆O₈SSi

Base Information

Chemical Name:C₃₈H₄₆O₈SSi
CAS No.:1174917-95-3
Molecular Formula:C₃₈H₄₆O₈SSi
Molecular Weight:690.93
Hs Code.:

C<sub>38</sub>H<sub>46</sub>O<sub>8</sub>SSi

Synonyms:C₃₈H₄₆O₈SSi

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Chemical Property of C₃₈H₄₆O₈SSi

Chemical Property:

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Technology Process of C₃₈H₄₆O₈SSi

There total 10 articles about C₃₈H₄₆O₈SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5-O-(tert-butyldiphenylsilyl)-4-C-((S)-1-hydroxyethyl)-1,2-O-isopropylidene-3-O-(2-naphthylmethyl)-α-D-ribofuranose

: 124-63-0
methanesulfonyl chloride

: 1174917-95-3
C₃₈H₄₆O₈SSi

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 ℃;
DOI:10.1021/jo902560f

Reference yield:

: 1070968-94-3
C₂₀H₂₄O₆

: 1174917-95-3
C₃₈H₄₆O₈SSi

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium periodate / 1,4-dioxane; water / 1.67 h

2.1: sodium hydroxide; water / tetrahydrofuran / 72 h / 20 °C / Cooling with ice

3.1: triethylamine / dichloromethane / 16 h / 0 - 20 °C

4.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

4.2: 1 h / -78 - 20 °C

5.1: cerium(III) chloride / tetrahydrofuran / 1.58 h / 0 °C

5.2: 3 h / -78 °C

5.3: 20 °C

6.1: triethylamine / dmap / dichloromethane / 2.5 h / 0 °C

With sodium periodate; cerium(III) chloride; oxalyl dichloride; water; dimethyl sulfoxide; triethylamine; sodium hydroxide; dmap; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water;

Reference yield:

: 3-O-(naphthalene-2-ylmethyl)-1,2;5,6-0-di(isopropylidene)-α-D-allofuranose

: 1174917-95-3
C₃₈H₄₆O₈SSi

Guidance literature:: Multi-step reaction with 7 steps

1.1: water; acetic acid / 16 h / 20 °C

2.1: sodium periodate / 1,4-dioxane; water / 1.67 h

3.1: sodium hydroxide; water / tetrahydrofuran / 72 h / 20 °C / Cooling with ice

4.1: triethylamine / dichloromethane / 16 h / 0 - 20 °C

5.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

5.2: 1 h / -78 - 20 °C

6.1: cerium(III) chloride / tetrahydrofuran / 1.58 h / 0 °C

6.2: 3 h / -78 °C

6.3: 20 °C

7.1: triethylamine / dmap / dichloromethane / 2.5 h / 0 °C

With sodium periodate; cerium(III) chloride; oxalyl dichloride; water; acetic acid; dimethyl sulfoxide; triethylamine; sodium hydroxide; dmap; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water;