methyl N-[2-(2-bromo-4,5-dimethoxyphenyl)ethyl]carbamate

Base Information

Chemical Name:methyl N-[2-(2-bromo-4,5-dimethoxyphenyl)ethyl]carbamate
CAS No.:74054-31-2
Molecular Formula:C12H16 Br N O4
Molecular Weight:318.167
Hs Code.:
NSC Number:143411
DSSTox Substance ID:DTXSID70995510
Wikidata:Q82986958

Synonyms:74054-31-2;NSC143411;DTXSID70995510;NSC-143411;Methyl hydrogen [2-(2-bromo-4,5-dimethoxyphenyl)ethyl]carbonimidate

Suppliers and Price of methyl N-[2-(2-bromo-4,5-dimethoxyphenyl)ethyl]carbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of methyl N-[2-(2-bromo-4,5-dimethoxyphenyl)ethyl]carbamate

Chemical Property:

Vapor Pressure:3.93E-07mmHg at 25°C
Boiling Point:416.1°C at 760 mmHg
Flash Point:205.4°C
Density:1.372g/cm³
XLogP3:2.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:6
Exact Mass:317.02627
Heavy Atom Count:18
Complexity:265

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=C(C(=C1)CCNC(=O)OC)Br)OC

Technology Process of methyl N-[2-(2-bromo-4,5-dimethoxyphenyl)ethyl]carbamate

There total 1 articles about methyl N-[2-(2-bromo-4,5-dimethoxyphenyl)ethyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.6%

: 35690-71-2
[2-(3,4-dimethoxy-phenyl)-ethyl]-carbamic acid methyl ester

: 74054-31-2
methyl 2-bromo-4,5-dimethoxyphenethylcarbamate

Guidance literature:: With bromine; In acetic acid; for 2h; Ambient temperature;
DOI:10.1039/P19810000290

Reference yield: 65.7%

: 74054-31-2
methyl 2-bromo-4,5-dimethoxyphenethylcarbamate

: 74054-32-3
2,3-dihydro-5,6-dimethoxy-1-methoxycarbonyl-1H-indole

Guidance literature:: With copper(l) iodide; sodium hydride; In N,N-dimethyl-formamide; 1.) room temperature, 30 min, 2.) 80 - 85 deg C, 12 h;
DOI:10.1039/P19810000290

Reference yield:

: 74054-31-2
methyl 2-bromo-4,5-dimethoxyphenethylcarbamate

: 14430-23-0
5,6-dimethoxyindole

Guidance literature:: Multi-step reaction with 3 steps

1: 65.7 percent / sodium hydride, cuprous iodide / dimethylformamide / 1.) room temperature, 30 min, 2.) 80 - 85 deg C, 12 h

2: 88.1 percent / manganese dioxide / CH₂Cl₂ / 72 h / Ambient temperature

3: 71.9 percent / Claisen's alkali / 0.5 h / Heating

With manganese(IV) oxide; copper(l) iodide; Claisen's alkali; sodium hydride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/P19810000290