N-methoxymethyl-N-(N-trifluoroacetyl-4-methoxymethoxy-1-prolyl)-2-bromo-4-methoxy-5-tosyloxyaniline

Base Information

Chemical Name:N-methoxymethyl-N-(N-trifluoroacetyl-4-methoxymethoxy-1-prolyl)-2-bromo-4-methoxy-5-tosyloxyaniline
CAS No.:105823-08-3
Molecular Formula:C₂₅H₂₈BrF₃N₂O₉S
Molecular Weight:669.471
Hs Code.:

Synonyms:N-methoxymethyl-N-(N-trifluoroacetyl-4-methoxymethoxy-1-prolyl)-2-bromo-4-methoxy-5-tosyloxyaniline

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Chemical Property of N-methoxymethyl-N-(N-trifluoroacetyl-4-methoxymethoxy-1-prolyl)-2-bromo-4-methoxy-5-tosyloxyaniline

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Technology Process of N-methoxymethyl-N-(N-trifluoroacetyl-4-methoxymethoxy-1-prolyl)-2-bromo-4-methoxy-5-tosyloxyaniline

There total 5 articles about N-methoxymethyl-N-(N-trifluoroacetyl-4-methoxymethoxy-1-prolyl)-2-bromo-4-methoxy-5-tosyloxyaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 107-30-2
chloromethyl methyl ether

: 105823-07-2
N-(4-hydroxy-1-trifluoroacetyl-1-prolyl)-2-bromo-4-methoxy-5-tosyloxy-aniline

: 105823-08-3
N-methoxymethyl-N-(N-trifluoroacetyl-4-methoxymethoxy-1-prolyl)-2-bromo-4-methoxy-5-tosyloxyaniline

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; for 120h;
DOI:10.1016/S0040-4020(01)87534-7

Reference yield:

: 83577-93-9
(2S,4R)-N-trifluoroacetyl-4-[(trifluoroacetyl)oxy]proline

: 105823-08-3
N-methoxymethyl-N-(N-trifluoroacetyl-4-methoxymethoxy-1-prolyl)-2-bromo-4-methoxy-5-tosyloxyaniline

Guidance literature:: Multi-step reaction with 3 steps

2: aq. NaHCO₃

3: di-isopropylethylamine

With sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine;
DOI:10.1039/c39860000841

Reference yield:

: 89625-38-7
2-bromo-4-methoxy-5-tosyloxyaniline

: 105823-08-3
N-methoxymethyl-N-(N-trifluoroacetyl-4-methoxymethoxy-1-prolyl)-2-bromo-4-methoxy-5-tosyloxyaniline

Guidance literature:: Multi-step reaction with 3 steps

2: aq. NaHCO₃

3: di-isopropylethylamine

With sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine;
DOI:10.1039/c39860000841