(S)-3-Benzyloxycarbonylamino-N-[(R)-1-((S)-1-phenyl-propylcarbamoyl)-propyl]-succinamic acid

Base Information

Chemical Name:(S)-3-Benzyloxycarbonylamino-N-[(R)-1-((S)-1-phenyl-propylcarbamoyl)-propyl]-succinamic acid
CAS No.:189878-78-2
Molecular Formula:C₂₅H₃₁N₃O₆
Molecular Weight:469.538
Hs Code.:

Synonyms:(S)-3-Benzyloxycarbonylamino-N-[(R)-1-((S)-1-phenyl-propylcarbamoyl)-propyl]-succinamic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-3-Benzyloxycarbonylamino-N-[(R)-1-((S)-1-phenyl-propylcarbamoyl)-propyl]-succinamic acid

Chemical Property:

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Technology Process of (S)-3-Benzyloxycarbonylamino-N-[(R)-1-((S)-1-phenyl-propylcarbamoyl)-propyl]-succinamic acid

There total 2 articles about (S)-3-Benzyloxycarbonylamino-N-[(R)-1-((S)-1-phenyl-propylcarbamoyl)-propyl]-succinamic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 135841-16-6
(R)-3-benzyloxycarbonyl-5-oxo-4-oxazolidinoneacetic acid

: 176641-94-4
D-2-Aminobutyric acid (S)-α-phenylpropylamide

: 189878-78-2
(S)-3-Benzyloxycarbonylamino-N-[(R)-1-((S)-1-phenyl-propylcarbamoyl)-propyl]-succinamic acid

: (S)-3-(Benzyloxycarbonyl-hydroxymethyl-amino)-N-[(R)-1-((S)-1-phenyl-propylcarbamoyl)-propyl]-succinamic acid

Guidance literature:: With triethylamine; In acetonitrile; at 40 ℃; for 24h; Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1080/00304949709355181

Reference yield:

: 135841-16-6
(R)-3-benzyloxycarbonyl-5-oxo-4-oxazolidinoneacetic acid

: 176641-94-4
D-2-Aminobutyric acid (S)-α-phenylpropylamide

: 189878-78-2
(S)-3-Benzyloxycarbonylamino-N-[(R)-1-((S)-1-phenyl-propylcarbamoyl)-propyl]-succinamic acid

Guidance literature:: With sodium carbonate; triethylamine; Yield given. Multistep reaction; 1.) CH₃CN, 40 deg C, 24 h, 2.) MeOH, 30 deg C, 24 h;
DOI:10.1080/00304949709355181

Reference yield:

: 189878-78-2
(S)-3-Benzyloxycarbonylamino-N-[(R)-1-((S)-1-phenyl-propylcarbamoyl)-propyl]-succinamic acid

: L-aspartyl-D-α-aminobutyric acid (S)-α-ethylbenzylamide

: β-L-Aspartyl-D-2-aminobutyric acid (S)-α-phenylpropylamide

: L-Aspartyl-L-2-aminobutyric acid (S)-α-phenylpropylamide

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; water; for 8h; under 2068.6 Torr; Ambient temperature;
DOI:10.1080/00304949709355181