D-2-Aminobutyric acid (S)-α-phenylpropylamide

Base Information

Chemical Name:D-2-Aminobutyric acid (S)-α-phenylpropylamide
CAS No.:176641-94-4
Molecular Formula:C₁₃H₂₀N₂O
Molecular Weight:220.315
Hs Code.:

Synonyms:D-2-Aminobutyric acid (S)-α-phenylpropylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of D-2-Aminobutyric acid (S)-α-phenylpropylamide

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Technology Process of D-2-Aminobutyric acid (S)-α-phenylpropylamide

There total 1 articles about D-2-Aminobutyric acid (S)-α-phenylpropylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 189878-81-7
[(R)-1-((S)-1-Phenyl-propylcarbamoyl)-propyl]-carbamic acid benzyl ester

: 176641-94-4
D-2-Aminobutyric acid (S)-α-phenylpropylamide

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; water; under 1810.02 - 2068.6 Torr;
DOI:10.1080/00304949709355181

Reference yield:

: 176641-94-4
D-2-Aminobutyric acid (S)-α-phenylpropylamide

: L-aspartyl-D-α-aminobutyric acid (S)-α-ethylbenzylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Et₃N, 2.) 5percent aq. Na₂CO₃ / 1.) CH₃CN, 40 deg C, 24 h, 2.) MeOH, 30 deg C, 24 h

2: 91 percent / H₂ / 10percent Pd/C / methanol; H₂O / 8 h / 2068.6 Torr / Ambient temperature

With hydrogen; sodium carbonate; triethylamine; palladium on activated charcoal; In methanol; water;
DOI:10.1080/00304949709355181

Reference yield:

: 176641-94-4
D-2-Aminobutyric acid (S)-α-phenylpropylamide

: β-L-Aspartyl-D-2-aminobutyric acid (S)-α-phenylpropylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Et₃N, 2.) 5percent aq. Na₂CO₃ / 1.) CH₃CN, 40 deg C, 24 h, 2.) MeOH, 30 deg C, 24 h

2: 3.4 percent Chromat_. / H₂ / 10percent Pd/C / methanol; H₂O / 8 h / 2068.6 Torr / Ambient temperature

With hydrogen; sodium carbonate; triethylamine; palladium on activated charcoal; In methanol; water;
DOI:10.1080/00304949709355181