2-(6,7-dimethoxy-1-oxo-2-vinyl-1,2-dihydroisoquinolin-3-yl)-4,5-dimethoxybenzaldehyde

Base Information

Chemical Name:2-(6,7-dimethoxy-1-oxo-2-vinyl-1,2-dihydroisoquinolin-3-yl)-4,5-dimethoxybenzaldehyde
CAS No.:1202036-75-6
Molecular Formula:C₂₂H₂₁NO₆
Molecular Weight:395.412
Hs Code.:

Synonyms:2-(6,7-dimethoxy-1-oxo-2-vinyl-1,2-dihydroisoquinolin-3-yl)-4,5-dimethoxybenzaldehyde

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Chemical Property of 2-(6,7-dimethoxy-1-oxo-2-vinyl-1,2-dihydroisoquinolin-3-yl)-4,5-dimethoxybenzaldehyde

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Technology Process of 2-(6,7-dimethoxy-1-oxo-2-vinyl-1,2-dihydroisoquinolin-3-yl)-4,5-dimethoxybenzaldehyde

There total 1 articles about 2-(6,7-dimethoxy-1-oxo-2-vinyl-1,2-dihydroisoquinolin-3-yl)-4,5-dimethoxybenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1202036-70-1
C₂₂H₂₃NO₆

: 1202036-75-6
2-(6,7-dimethoxy-1-oxo-2-vinyl-1,2-dihydroisoquinolin-3-yl)-4,5-dimethoxybenzaldehyde

Guidance literature:: With dipyridinium dichromate; In dichloromethane; for 2h;
DOI:10.1016/j.tet.2009.10.027

Reference yield: 53.0%

: 1202036-75-6
2-(6,7-dimethoxy-1-oxo-2-vinyl-1,2-dihydroisoquinolin-3-yl)-4,5-dimethoxybenzaldehyde

: 1779-49-3
Methyltriphenylphosphonium bromide

: 1202036-80-3
3-(4,5-dimethoxy-2-vinylphenyl)-6,7-dimethoxy-2-vinyl-2H-isoquinolin-1-one

Guidance literature:: Methyltriphenylphosphonium bromide; With n-butyllithium; In tetrahydrofuran; hexane; at 0 ℃; for 1h;

2-(6,7-dimethoxy-1-oxo-2-vinyl-1,2-dihydroisoquinolin-3-yl)-4,5-dimethoxybenzaldehyde; In tetrahydrofuran; hexane; at 0 - 20 ℃;
DOI:10.1016/j.tet.2009.10.027