1,2,3,4-tetrahydro-6,7-dimethoxy-3-Isoquinolinecarboxylic acid methyl ester

Base Information

Chemical Name:1,2,3,4-tetrahydro-6,7-dimethoxy-3-Isoquinolinecarboxylic acid methyl ester
CAS No.:88932-16-5
Molecular Formula:C₁₃H₁₇NO₄
Molecular Weight:251.282
Hs Code.:

Synonyms:1,2,3,4-tetrahydro-6,7-dimethoxy-3-Isoquinolinecarboxylic acid methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2,3,4-tetrahydro-6,7-dimethoxy-3-Isoquinolinecarboxylic acid methyl ester

Chemical Property:

Purity/Quality:

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Technology Process of 1,2,3,4-tetrahydro-6,7-dimethoxy-3-Isoquinolinecarboxylic acid methyl ester

There total 1 articles about 1,2,3,4-tetrahydro-6,7-dimethoxy-3-Isoquinolinecarboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 32161-30-1
(S)-3,4-dimethoxyphenylalanine

: 88932-16-5
1,2,3,4-tetrahydro-6,7-dimethoxy-3-Isoquinolinecarboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 20 °C

2: trifluoroacetic acid / methanol / 6 h / 40 °C

With thionyl chloride; trifluoroacetic acid; In methanol;
DOI:10.1002/ejoc.201801147

Reference yield: 45.0%

: 5153-67-3
nitrostyrene

: 88932-16-5
1,2,3,4-tetrahydro-6,7-dimethoxy-3-Isoquinolinecarboxylic acid methyl ester

: Methyl 2,3-dimethoxy-6-nitro-7-phenyl-5,6,7,9-tetrahydro-8H-5,8-epiminobenzo [7]annulene-8-carboxylate

Guidance literature:: With palladium on activated charcoal; In toluene; at 70 ℃; for 36h; diastereoselective reaction; Schlenk technique; Sealed tube; Inert atmosphere;
DOI:10.1002/ejoc.201801147

Reference yield:

: 1083-11-0
4-(2,5-dimethoxyphenyl)butyric acid

: 88932-16-5
1,2,3,4-tetrahydro-6,7-dimethoxy-3-Isoquinolinecarboxylic acid methyl ester

: 1326317-19-4
methyl 2-(4-(2,5-dimethoxyphenyl)butanoyl)-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline-3-carboxylate

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1021/jm2008387