Technology Process of C28H29NO2S
There total 4 articles about C28H29NO2S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
trifuran-2-yl-phosphane; potassium acetate; bis(dibenzylideneacetone)-palladium(0);
In
N,N-dimethyl-formamide;
at 85 ℃;
for 4h;
Inert atmosphere;
DOI:10.1021/jo202590w
- Guidance literature:
-
Multi-step reaction with 2 steps
1: pyridine / dichloromethane / 2.5 h / 0 °C
2: trifuran-2-yl-phosphane; potassium acetate; bis(dibenzylideneacetone)-palladium(0) / N,N-dimethyl-formamide / 4 h / 85 °C / Inert atmosphere
With
pyridine; trifuran-2-yl-phosphane; potassium acetate; bis(dibenzylideneacetone)-palladium(0);
In
dichloromethane; N,N-dimethyl-formamide;
2: Suzuki coupling;
DOI:10.1021/jo202590w
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: ethylmagnesium bromide / tetrahydrofuran / 1 h / 50 °C
1.2: 3 h / 20 °C
2.1: pyridine / dichloromethane / 2.5 h / 0 °C
3.1: trifuran-2-yl-phosphane; potassium acetate; bis(dibenzylideneacetone)-palladium(0) / N,N-dimethyl-formamide / 4 h / 85 °C / Inert atmosphere
With
pyridine; trifuran-2-yl-phosphane; ethylmagnesium bromide; potassium acetate; bis(dibenzylideneacetone)-palladium(0);
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
3.1: Suzuki coupling;
DOI:10.1021/jo202590w
