(E)-N-[2-(3-N'-phenylhydrazonoprop-1-enyl)phenyl]-2-amino-1,4-naphthoquinone

Base Information

Chemical Name:(E)-N-[2-(3-N'-phenylhydrazonoprop-1-enyl)phenyl]-2-amino-1,4-naphthoquinone
CAS No.:460041-71-8
Molecular Formula:C₂₅H₁₉N₃O₂
Molecular Weight:393.445
Hs Code.:

Synonyms:(E)-N-[2-(3-N'-phenylhydrazonoprop-1-enyl)phenyl]-2-amino-1,4-naphthoquinone

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Chemical Property of (E)-N-[2-(3-N'-phenylhydrazonoprop-1-enyl)phenyl]-2-amino-1,4-naphthoquinone

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Technology Process of (E)-N-[2-(3-N'-phenylhydrazonoprop-1-enyl)phenyl]-2-amino-1,4-naphthoquinone

There total 4 articles about (E)-N-[2-(3-N'-phenylhydrazonoprop-1-enyl)phenyl]-2-amino-1,4-naphthoquinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 59-88-1
phenylhydrazine hydrochloride

: 460041-64-9
(E)-N-[2-(3-oxoprop-1-enyl)phenyl]-2-amino-1,4-naphthoquinone

: 460041-71-8
(E)-N-[2-(3-N'-phenylhydrazonoprop-1-enyl)phenyl]-2-amino-1,4-naphthoquinone

Guidance literature:: With dmap; In ethanol; at 23 ℃; for 0.5h;
DOI:10.1039/b202555h

Reference yield:

: 1504-65-0,130489-97-3
2-nitrocinnamyl alcohol

: 460041-71-8
(E)-N-[2-(3-N'-phenylhydrazonoprop-1-enyl)phenyl]-2-amino-1,4-naphthoquinone

Guidance literature:: Multi-step reaction with 4 steps

1: 77 percent / FeSO₄*7H₂O; aq. NH₄OH / methanol / 3 h / 80 °C

2: 70 percent / CeCl₃*7H₂O; O₂ / methanol / 24 h / 23 °C

3: 66 percent / PCC / CH₂Cl₂ / 2 h / 23 °C

4: 77 percent / DMAP / ethanol / 0.5 h / 23 °C

With dmap; ammonium hydroxide; cerium(III) chloride; oxygen; iron(II) sulfate; pyridinium chlorochromate; In methanol; ethanol; dichloromethane; 2: Michael addition;
DOI:10.1039/b202555h

Reference yield:

: 195191-58-3
(E)-3-(2-aminophenyl)prop-2-en-1-ol

: 460041-71-8
(E)-N-[2-(3-N'-phenylhydrazonoprop-1-enyl)phenyl]-2-amino-1,4-naphthoquinone

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / CeCl₃*7H₂O; O₂ / methanol / 24 h / 23 °C

2: 66 percent / PCC / CH₂Cl₂ / 2 h / 23 °C

3: 77 percent / DMAP / ethanol / 0.5 h / 23 °C

With dmap; cerium(III) chloride; oxygen; pyridinium chlorochromate; In methanol; ethanol; dichloromethane; 1: Michael addition;
DOI:10.1039/b202555h