(1R,2R)-N,N'-bisformyl-N,N'-bis(2,3-dimethylbenzyl)-1,2-cyclohexanediamine

Base Information

Chemical Name:(1R,2R)-N,N'-bisformyl-N,N'-bis(2,3-dimethylbenzyl)-1,2-cyclohexanediamine
CAS No.:1374787-77-5
Molecular Formula:C₂₆H₃₄N₂O₂
Molecular Weight:406.568
Hs Code.:

Synonyms:(1R,2R)-N,N'-bisformyl-N,N'-bis(2,3-dimethylbenzyl)-1,2-cyclohexanediamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,2R)-N,N'-bisformyl-N,N'-bis(2,3-dimethylbenzyl)-1,2-cyclohexanediamine

Chemical Property:

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Technology Process of (1R,2R)-N,N'-bisformyl-N,N'-bis(2,3-dimethylbenzyl)-1,2-cyclohexanediamine

There total 3 articles about (1R,2R)-N,N'-bisformyl-N,N'-bis(2,3-dimethylbenzyl)-1,2-cyclohexanediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₄H₃₄N₂

: 2258-42-6
formyl acetic anhydride

: 1374787-77-5
(1R,2R)-N,N'-bisformyl-N,N'-bis(2,3-dimethylbenzyl)-1,2-cyclohexanediamine

Guidance literature:: In dichloromethane; at 0 - 20 ℃; for 24h;
DOI:10.1016/j.tetasy.2012.02.015

Reference yield:

: 5779-93-1
2,3-dimethylbenzaldehyde

: 1374787-77-5
(1R,2R)-N,N'-bisformyl-N,N'-bis(2,3-dimethylbenzyl)-1,2-cyclohexanediamine

Guidance literature:: Multi-step reaction with 3 steps

1: amberlyst 15 / toluene / 12 h / Molecular sieve; Inert atmosphere; Reflux

2: sodium tetrahydroborate / methanol / 20 h / 0 - 20 °C

3: dichloromethane / 24 h / 0 - 20 °C

With sodium tetrahydroborate; In methanol; dichloromethane; toluene;
DOI:10.1016/j.tetasy.2012.02.015

Reference yield:

: 20439-47-8
(1R,2R)-1,2-diaminocyclohexane

: 1374787-77-5
(1R,2R)-N,N'-bisformyl-N,N'-bis(2,3-dimethylbenzyl)-1,2-cyclohexanediamine

Guidance literature:: Multi-step reaction with 3 steps

1: amberlyst 15 / toluene / 12 h / Molecular sieve; Inert atmosphere; Reflux

2: sodium tetrahydroborate / methanol / 20 h / 0 - 20 °C

3: dichloromethane / 24 h / 0 - 20 °C

With sodium tetrahydroborate; In methanol; dichloromethane; toluene;
DOI:10.1016/j.tetasy.2012.02.015