(1,3-bis(2,6-diisopropylphenyl)-4,5,6,7-tetrahydro-3H-[1,3]diazepin-1-ium)BF₄

Base Information

Chemical Name:(1,3-bis(2,6-diisopropylphenyl)-4,5,6,7-tetrahydro-3H-[1,3]diazepin-1-ium)BF₄
CAS No.:1034137-39-7
Molecular Formula:BF₄*C₂₉H₄₃N₂
Molecular Weight:506.478
Hs Code.:

(1,3-bis(2,6-diisopropylphenyl)-4,5,6,7-tetrahydro-3H-[1,3]diazepin-1-ium)BF<sub>4</sub>

Synonyms:(1,3-bis(2,6-diisopropylphenyl)-4,5,6,7-tetrahydro-3H-[1,3]diazepin-1-ium)BF₄

Suppliers and Price of (1,3-bis(2,6-diisopropylphenyl)-4,5,6,7-tetrahydro-3H-[1,3]diazepin-1-ium)BF₄

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (1,3-bis(2,6-diisopropylphenyl)-4,5,6,7-tetrahydro-3H-[1,3]diazepin-1-ium)BF₄

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (1,3-bis(2,6-diisopropylphenyl)-4,5,6,7-tetrahydro-3H-[1,3]diazepin-1-ium)BF₄

There total 2 articles about (1,3-bis(2,6-diisopropylphenyl)-4,5,6,7-tetrahydro-3H-[1,3]diazepin-1-ium)BF₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110-52-1
1,4-dibromo-butane

: 1176938-29-6,581776-24-1
N,N'-di(2,6-diisopropylphenyl)formamidine

: 1034137-39-7
(1,3-bis(2,6-diisopropylphenyl)-4,5,6,7-tetrahydro-3H-[1,3]diazepin-1-ium)BF₄

Guidance literature:: With sodium tetrafluoroborate; potassium carbonate; N-ethyl-N,N-diisopropylamine; In dichloromethane; water; acetone; toluene; at 120 ℃; for 1h; Heating; Inert atmosphere;
DOI:10.1039/c3dt32860k

Reference yield:

: 24544-04-5
2,6-diisopropylbenzenamine

: 1034137-39-7
(1,3-bis(2,6-diisopropylphenyl)-4,5,6,7-tetrahydro-3H-[1,3]diazepin-1-ium)BF₄

Guidance literature:: Multi-step reaction with 2 steps

1: 20 °C

2: sodium tetrafluoroborate; potassium carbonate; N-ethyl-N,N-diisopropylamine / toluene; dichloromethane; acetone; water / 1 h / 120 °C / Heating; Inert atmosphere

With sodium tetrafluoroborate; potassium carbonate; N-ethyl-N,N-diisopropylamine; In dichloromethane; water; acetone; toluene;
DOI:10.1039/c3dt32860k

Reference yield: 79.0%

: 1034137-39-7
(1,3-bis(2,6-diisopropylphenyl)-4,5,6,7-tetrahydro-3H-[1,3]diazepin-1-ium)BF₄

: copper(l) chloride

: [(1,3-bis(2,6-diisopropylphenyl)-4,5,6,7-tetrahydro-1,3-diazepin-2-ylidene)CuCl]

Guidance literature:: (1,3-bis(2,6-diisopropylphenyl)-4,5,6,7-tetrahydro-3H-[1,3]diazepin-1-ium)BF₄; With sodium hexamethyldisilazane; In tetrahydrofuran; for 2h; Inert atmosphere;

copper(l) chloride; In tetrahydrofuran; Inert atmosphere; Schlenk technique;
DOI:10.1021/acs.organomet.6b00025