6-(tert-butyl-diphenyl-silanyloxy)-4,4-dimethyl-1-(1-methyl-cyclohexa-2,5-dienyl)-hex-1-en-3-ol

Base Information

Chemical Name:6-(tert-butyl-diphenyl-silanyloxy)-4,4-dimethyl-1-(1-methyl-cyclohexa-2,5-dienyl)-hex-1-en-3-ol
CAS No.:235434-15-8
Molecular Formula:C₃₁H₄₂O₂Si
Molecular Weight:474.759
Hs Code.:

6-(<i>tert</i>-butyl-diphenyl-silanyloxy)-4,4-dimethyl-1-(1-methyl-cyclohexa-2,5-dienyl)-hex-1-en-3-ol

Synonyms:6-(tert-butyl-diphenyl-silanyloxy)-4,4-dimethyl-1-(1-methyl-cyclohexa-2,5-dienyl)-hex-1-en-3-ol

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Chemical Property of 6-(tert-butyl-diphenyl-silanyloxy)-4,4-dimethyl-1-(1-methyl-cyclohexa-2,5-dienyl)-hex-1-en-3-ol

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Technology Process of 6-(tert-butyl-diphenyl-silanyloxy)-4,4-dimethyl-1-(1-methyl-cyclohexa-2,5-dienyl)-hex-1-en-3-ol

There total 1 articles about 6-(tert-butyl-diphenyl-silanyloxy)-4,4-dimethyl-1-(1-methyl-cyclohexa-2,5-dienyl)-hex-1-en-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 181576-39-6
3-[(Z)-2-Iodovinyl]-3-methylcyclohexa-1,4-diene

: 187869-61-0
4-(tert-butyldiphenysilanyloxy)-2,2-dimethylbutyraldehyde

: 235434-15-8
6-(tert-butyl-diphenyl-silanyloxy)-4,4-dimethyl-1-(1-methyl-cyclohexa-2,5-dienyl)-hex-1-en-3-ol

Guidance literature:: With tert.-butyl lithium; In tetrahydrofuran; at -78 ℃;
DOI:10.1039/a901392j

Reference yield: 96.0%

: 235434-15-8
6-(tert-butyl-diphenyl-silanyloxy)-4,4-dimethyl-1-(1-methyl-cyclohexa-2,5-dienyl)-hex-1-en-3-ol

: 74-88-4
methyl iodide

: 235434-16-9
tert-butyl-[4-methoxy-3,3-dimethyl-6-(1-methyl-cyclohexa-2,5-dienyl)-hex-5-enyloxy]-diphenyl-silane

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃;
DOI:10.1039/a901392j

Reference yield:

: 235434-15-8
6-(tert-butyl-diphenyl-silanyloxy)-4,4-dimethyl-1-(1-methyl-cyclohexa-2,5-dienyl)-hex-1-en-3-ol

: 235434-17-0
(Z)-4-Methoxy-3,3-dimethyl-6-(1-methyl-cyclohexa-2,5-dienyl)-hex-5-en-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / NaH / dimethylformamide / 0 - 20 °C

2: 94 percent / TBAF / tetrahydrofuran / Ambient temperature

With tetrabutyl ammonium fluoride; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/a901392j