4-[3-(3,4-dimethoxy-phenyl)-4,5-dihydro-isoxazol-5-ylmethoxy]-3-methoxy-benzaldehyde

Base Information

Chemical Name:4-[3-(3,4-dimethoxy-phenyl)-4,5-dihydro-isoxazol-5-ylmethoxy]-3-methoxy-benzaldehyde
CAS No.:370865-86-4
Molecular Formula:C₂₀H₂₁NO₆
Molecular Weight:371.39
Hs Code.:

Synonyms:4-[3-(3,4-dimethoxy-phenyl)-4,5-dihydro-isoxazol-5-ylmethoxy]-3-methoxy-benzaldehyde

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Chemical Property of 4-[3-(3,4-dimethoxy-phenyl)-4,5-dihydro-isoxazol-5-ylmethoxy]-3-methoxy-benzaldehyde

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Technology Process of 4-[3-(3,4-dimethoxy-phenyl)-4,5-dihydro-isoxazol-5-ylmethoxy]-3-methoxy-benzaldehyde

There total 1 articles about 4-[3-(3,4-dimethoxy-phenyl)-4,5-dihydro-isoxazol-5-ylmethoxy]-3-methoxy-benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 22280-95-1
4-allyloxy-3-methoxybenzaldehyde

: 2169-98-4,39627-82-2
3,4-Dimethoxy-benzaldehyde oxime

: 370865-86-4
4-[3-(3,4-dimethoxy-phenyl)-4,5-dihydro-isoxazol-5-ylmethoxy]-3-methoxy-benzaldehyde

Guidance literature:: With sodium hypochlorite; In dichloromethane; at 0 ℃; for 5h;
DOI:10.1016/S0040-4039(01)01126-1

Reference yield: 96.0%

: 370865-86-4
4-[3-(3,4-dimethoxy-phenyl)-4,5-dihydro-isoxazol-5-ylmethoxy]-3-methoxy-benzaldehyde

: 4-[3-(3,4-dimethoxy-phenyl)-4,5-dihydro-isoxazol-5-ylmethoxy]-3-methoxy-benzaldehyde oxime

Guidance literature:: With sodium hydroxide; hydroxylamine hydrochloride; In ethanol; for 14h; Heating;
DOI:10.1016/S0040-4039(01)01126-1

Reference yield:

: 370865-86-4
4-[3-(3,4-dimethoxy-phenyl)-4,5-dihydro-isoxazol-5-ylmethoxy]-3-methoxy-benzaldehyde

: 3-{4-[3-(3,4-dimethoxy-phenyl)-4,5-dihydro-isoxazol-5-ylmethoxy]-3-methoxy-phenyl}-5-phenyl-isoxazole

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / NH₂OH*HCl; NaOH / ethanol / 14 h / Heating

2: 70 percent / NaOCl / CH₂Cl₂ / 5 h / 0 °C

With sodium hydroxide; sodium hypochlorite; hydroxylamine hydrochloride; In ethanol; dichloromethane;
DOI:10.1016/S0040-4039(01)01126-1