1,5-decalindione monoethylene ketal

Base Information

Chemical Name:1,5-decalindione monoethylene ketal
CAS No.:173778-10-4
Molecular Formula:C₁₂H₁₈O₃
Molecular Weight:210.273
Hs Code.:

Synonyms:1,5-decalindione monoethylene ketal

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Chemical Property of 1,5-decalindione monoethylene ketal

Chemical Property:

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Technology Process of 1,5-decalindione monoethylene ketal

There total 1 articles about 1,5-decalindione monoethylene ketal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13913-82-1
octahydronaphthalene-1,5-dione

: 107-21-1
ethylene glycol

: 7049-11-8
1,5-decalindione bis-ethylene ketal

: 173778-10-4
1,5-decalindione monoethylene ketal

Guidance literature:: With toluene-4-sulfonic acid; In benzene; Heating;
DOI:10.1021/ja952852i

Reference yield:

: 173778-10-4
1,5-decalindione monoethylene ketal

: (1S,4aR,5R,8aS)-5-Biphenyl-4-yl-1,2,3,4,4a,5,6,7,8,8a-decahydro-[1,2']binaphthalenyl

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) n-butyllithium, 3.) H₂

2: 1.) n-butyllithium / 1.) THF, 1 h, 2.) THF, 3 h

3: 1.) acetic anhydride, acetyl chloride, 2.) H₂, 3.) potassium tert-butoxide / 2.) 10percent Pd/C

With n-butyllithium; potassium tert-butylate; hydrogen; acetic anhydride; acetyl chloride; palladium on activated charcoal;
DOI:10.1021/ja952852i

Reference yield:

: 173778-10-4
1,5-decalindione monoethylene ketal

: (1S,4aS,5S,8aS)-5-Biphenyl-4-yl-1,2,3,4,4a,5,6,7,8,8a-decahydro-[1,2']binaphthalenyl

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) n-butyllithium, 3.) H₂

2: 1.) n-butyllithium / 1.) THF, 1 h, 2.) THF, 3 h

3: 1.) acetic anhydride, acetyl chloride, 2.) H₂, 3.) potassium tert-butoxide / 2.) 10percent Pd/C

With n-butyllithium; potassium tert-butylate; hydrogen; acetic anhydride; acetyl chloride; palladium on activated charcoal;
DOI:10.1021/ja952852i