Technology Process of C33H51N5O8Si2
There total 5 articles about C33H51N5O8Si2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: trimethylsilyl trifluoromethanesulfonate; DBN / acetonitrile / 21 h / 0 - 65 °C
2.1: sodium methylate / 24 h / 20 °C
3.1: pyridine / 16 h / 20 °C
4.1: pyridine / dichloromethane / 5 h / 20 °C
5.1: borane dimethyl sulphide complex / tetrahydrofuran / 3 h / 0 °C
5.2: 2 h / 0 - 20 °C
With
pyridine; borane dimethyl sulphide complex; trimethylsilyl trifluoromethanesulfonate; DBN; sodium methylate;
pyridine;
In
tetrahydrofuran; dichloromethane; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: pyridine / 16 h / 20 °C
2.1: pyridine / dichloromethane / 5 h / 20 °C
3.1: borane dimethyl sulphide complex / tetrahydrofuran / 3 h / 0 °C
3.2: 2 h / 0 - 20 °C
With
pyridine; borane dimethyl sulphide complex;
pyridine;
In
tetrahydrofuran; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: trimethylsilyl trifluoromethanesulfonate; DBN / acetonitrile / 21 h / 0 - 65 °C
2.1: sodium methylate / 24 h / 20 °C
3.1: pyridine / 16 h / 20 °C
4.1: pyridine / dichloromethane / 5 h / 20 °C
5.1: borane dimethyl sulphide complex / tetrahydrofuran / 3 h / 0 °C
5.2: 2 h / 0 - 20 °C
With
pyridine; borane dimethyl sulphide complex; trimethylsilyl trifluoromethanesulfonate; DBN; sodium methylate;
pyridine;
In
tetrahydrofuran; dichloromethane; acetonitrile;